NF EN ISO 1133-2

NF EN ISO 1133-2

February 2012
Standard Current

Plastics - Determination of the melt mass-flow rate (MFR) and melt volume-flow rate (MVR) of thermoplastics - Part 2 : method for materials sensitive to time-temperature history and/or moisture

ISO 1133-2:2011 specifies a procedure for the determination of the melt volume-flow rate (MVR) and melt mass-flow rate (MFR) of thermoplastic materials that exhibit a high rheological sensitivity to the time-temperature history experienced by the sample during the test and/or to moisture. It is possible that this method will not be appropriate for materials whose rheological behaviour is extremely affected during testing. MFR values can be determined by calculation from MVR measurements provided the melt density at the test temperature and pressure is known, or by measurement using a cutting device provided that the accuracy of the measurement is at least the same as that of the MVR measurement. The primary difference between ISO 1133-2:2011 and ISO 1133-1 is that ISO 1133-2:2011 specifies tighter tolerances on the temperature in the cylinder and on the time duration over which the material is subjected to that temperature. Thus the time-temperature history of the material is more tightly controlled and consequently, for materials that are likely to be affected by exposure to elevated temperatures, the variability of test results is reduced compared with whether the specifications of ISO 1133-1 were used. ISO 1133-2:2011 also provides information for preparation and handling of moisture sensitive materials that again are critical to obtaining repeatable, reproducible and accurate data. The test conditions for measurement of the MVR and MFR are often specified in the material standard. However, for those materials where there are no test conditions specified in the material standard, it is necessary for the test conditions to be agreed between the interested parties

View the extract
Main informations

Collections

National standards and national normative documents

Publication date

February 2012

Number of pages

24 p.

Reference

NF EN ISO 1133-2

ICS Codes

83.080.20   Thermoplastic materials

Classification index

T51-038-2

Print number

1 - 01/02/2012

International kinship

European kinship

EN ISO 1133-2:2011
Sumary
Plastics - Determination of the melt mass-flow rate (MFR) and melt volume-flow rate (MVR) of thermoplastics - Part 2 : method for materials sensitive to time-temperature history and/or moisture

ISO 1133-2:2011 specifies a procedure for the determination of the melt volume-flow rate (MVR) and melt mass-flow rate (MFR) of thermoplastic materials that exhibit a high rheological sensitivity to the time-temperature history experienced by the sample during the test and/or to moisture.

It is possible that this method will not be appropriate for materials whose rheological behaviour is extremely affected during testing.

MFR values can be determined by calculation from MVR measurements provided the melt density at the test temperature and pressure is known, or by measurement using a cutting device provided that the accuracy of the measurement is at least the same as that of the MVR measurement.

The primary difference between ISO 1133-2:2011 and ISO 1133-1 is that ISO 1133-2:2011 specifies tighter tolerances on the temperature in the cylinder and on the time duration over which the material is subjected to that temperature. Thus the time-temperature history of the material is more tightly controlled and consequently, for materials that are likely to be affected by exposure to elevated temperatures, the variability of test results is reduced compared with whether the specifications of ISO 1133-1 were used.

ISO 1133-2:2011 also provides information for preparation and handling of moisture sensitive materials that again are critical to obtaining repeatable, reproducible and accurate data.

The test conditions for measurement of the MVR and MFR are often specified in the material standard. However, for those materials where there are no test conditions specified in the material standard, it is necessary for the test conditions to be agreed between the interested parties

Table of contents
View the extract
  • Avant-propos
    iv
  • Introduction
    v
  • 1 Domaine d'application
    1
  • 2 Références normatives
    2
  • 3 Termes et définitions
    2
  • 4 Principe
    2
  • 5 Appareillage
    3
  • 5.1 Plastomètre d'extrusion
    3
  • 5.2 Équipement accessoire
    3
  • 6 Échantillon d'essai
    4
  • 6.1 Forme de l'échantillon
    4
  • 6.2 Prétraitement et stockage de l'échantillon
    4
  • 7 Vérification de la température, nettoyage et entretien de l'appareillage
    5
  • 7.1 Vérification du système de régulation de la température
    5
  • 7.2 Nettoyage de l'appareillage
    6
  • 7.3 Alignement vertical de l'instrument
    6
  • 8 Mode opératoire de montage
    6
  • 8.1 Généralités
    6
  • 8.2 Choix de la température et de la charge
    6
  • 8.3 Nettoyage
    6
  • 8.4 Choix de la masse de l'échantillon et chargement du cylindre
    7
  • 9 Mode opératoire
    8
  • 9.1 Choix de la température et de la charge
    8
  • 9.2 Distance de déplacement minimale du piston
    8
  • 9.3 Dispositif de chronométrage
    8
  • 9.4 Préparatifs pour l'essai
    8
  • 9.5 Mesurage
    8
  • 9.6 Expression des résultats
    9
  • 10 Rapport des vitesses d'écoulement (FRR)
    9
  • 11 Fidélité
    9
  • 12 Rapport d'essai
    9
  • Annexe A (informative) Vérification de la température dans le cylindre
    10
  • Annexe B (informative) Déterminations répétées de l'indice MVR sur différents matériaux effectuées conformément à la présente partie de l'ISO 1133
    14
  • Bibliographie
    16
ZOOM ON ... the Requirements department
To comply with a standard, you need to quickly understand its issues in order to determine its impact on your activity.

The Requirements department helps you quickly locate within the normative text:
- mandatory clauses to satisfy,
- non-essential but useful clauses to know, such as permissions and recommendations.

The identification of these types of clauses is based on the document “ISO / IEC Directives, Part 2 - Principles and rules of structure and drafting of ISO documents ”as well as on a constantly enriched list of verbal forms.

With Requirements, quickly access the main part of the normative text!

With Requirements, quickly access the main part of the normative text!
Need to identify, monitor and decipher standards?

COBAZ is the simple and effective solution to meet the normative needs related to your activity, in France and abroad.

Available by subscription, CObaz is THE modular solution to compose according to your needs today and tomorrow. Quickly discover CObaz!

Request your free, no-obligation live demo

I discover COBAZ