NF EN ISO 23631

NF EN ISO 23631

June 2006
Standard Current

Water quality - Determination of dalapon, trichloroacetic acid and selected haloacetic acids - Method using gas chromatography (GCD-ECD and/or GC-MS detection) after liquid-liquid extraction and derivatization

ISO 23631:2006 specifies a method for the determination of dalapon, trichloroacetic acid (TCA) and selected haloacetic acids in ground water and drinking water by gas chromatography (GC-ECD and/or GC-MS detection) after liquid-liquid-extraction and derivatization using diazomethane. Depending on the matrix, the method is applicable to a concentration range from 0,5 to 10 micrograms per litre. The validated reporting limit of TCA and dalapon is about 0,05 micrograms per litre. Detection by electron-capture detector (ECD) in general leads to lower detection limits. Detection by mass spectrometry (MS) allows analyte identification.

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Main informations

Collections

National standards and national normative documents

Publication date

June 2006

Number of pages

36 p.

Reference

NF EN ISO 23631

ICS Codes

13.060.50   Examination of water for chemical substances

Classification index

T90-182

Print number

2 - 01/03/2007

International kinship

European kinship

EN ISO 23631:2006
Sumary
Water quality - Determination of dalapon, trichloroacetic acid and selected haloacetic acids - Method using gas chromatography (GCD-ECD and/or GC-MS detection) after liquid-liquid extraction and derivatization

ISO 23631:2006 specifies a method for the determination of dalapon, trichloroacetic acid (TCA) and selected haloacetic acids in ground water and drinking water by gas chromatography (GC-ECD and/or GC-MS detection) after liquid-liquid-extraction and derivatization using diazomethane. Depending on the matrix, the method is applicable to a concentration range from 0,5 to 10 micrograms per litre. The validated reporting limit of TCA and dalapon is about 0,05 micrograms per litre. Detection by electron-capture detector (ECD) in general leads to lower detection limits. Detection by mass spectrometry (MS) allows analyte identification.

Table of contents
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  • Avant-propos
    iv
  • Introduction
    v
  • 1 Domaine d'application
    1
  • 2 Références normatives
    2
  • 3 Principe
    2
  • 4 Interférences
    2
  • 5 Réactifs
    2
  • 6 Appareillage
    5
  • 7 Échantillonnage et prétraitement des échantillons
    7
  • 8 Mode opératoire
    7
  • 9 Étalonnage
    10
  • 10 Calculs
    13
  • 11 Expression des résultats
    14
  • 12 Rapport d'essai
    15
  • Annexe A (informative) Exemples de chromatogrammes en phase gazeuse
    16
  • Annexe B (informative) Spectres de masse du dalapon méthylé et d'acides haloacétiques
    19
  • Annexe C (informative) Données de fidélité
    23
  • Bibliographie
    24
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