NF EN ISO 4259

NF EN ISO 4259

November 2006
Standard Cancelled mandatory application standard

Petroleum products - Determination and application of precision data in relation to methods of test

ISO 4259:2006 covers the calculation of precision estimates and their application to specifications. In particular, it contains definitions of relevant statistical terms, the procedures to be adopted in the planning of an inter-laboratory test programme to determine the precision of a test method, the method of calculating the precision from the results of such a programme, and the procedure to be followed in the interpretation of laboratory results in relation both to precision of the test methods and to the limits laid down in specifications. The procedures in ISO 4259:2006 have been designed specifically for petroleum and petroleum-related products, which are normally homogeneous. However, the procedures described in this International Standard can also be applied to other types of homogeneous products. Careful investigations are necessary before applying ISO 4259:2006 to products for which the assumption of homogeneity can be questioned.

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Main informations

Collections

National standards and national normative documents

Publication date

November 2006

Number of pages

72 p.

Reference

NF EN ISO 4259

ICS Codes

75.080   Petroleum products in general

Classification index

M07-033

Print number

1 - 13/11/2006

International kinship

European kinship

EN ISO 4259:2006
Sumary
Petroleum products - Determination and application of precision data in relation to methods of test

ISO 4259:2006 covers the calculation of precision estimates and their application to specifications. In particular, it contains definitions of relevant statistical terms, the procedures to be adopted in the planning of an inter-laboratory test programme to determine the precision of a test method, the method of calculating the precision from the results of such a programme, and the procedure to be followed in the interpretation of laboratory results in relation both to precision of the test methods and to the limits laid down in specifications.

The procedures in ISO 4259:2006 have been designed specifically for petroleum and petroleum-related products, which are normally homogeneous. However, the procedures described in this International Standard can also be applied to other types of homogeneous products. Careful investigations are necessary before applying ISO 4259:2006 to products for which the assumption of homogeneity can be questioned.

Replaced standards (1)
NF EN ISO 4259
December 1995
Standard Cancelled
Petroleum products. Determination and application of precision data in relation to methods of test.

Standard replaced by (2)
NF EN ISO 4259-2
December 2017
Standard Current
Petroleum and related products - Precision of measurement methods and results - Part 2 : interpretation and application of precision data in relation to methods of test

<p>ISO 4259-2:2017 specifies the methodology for the application of precision estimates of a test method derived from ISO 4259‑1. In particular, it defines the procedures for setting the property specification limits based upon test method precision where the property is determined using a specific test method, and in determining the specification conformance status when there are conflicting results between supplier and receiver. Other applications of this test method precision are briefly described in principle without the associated procedures.</p> <p>The procedures in ISO 4259-2:2017 have been designed specifically for petroleum and petroleum-related products, which are normally homogeneous. However, the procedures described in ISO 4259-2:2017 can also be applied to other types of homogeneous products. Careful investigations are necessary before applying ISO 4259-2:2017 to products for which the assumption of homogeneity can be questioned.</p>

NF EN ISO 4259-1
December 2017
Standard Current
Petroleum and related products - Precision of measurement methods and results - Part 1 : determination of precision data in relation to methods of test

<p>ISO 4259-1:2017 specifies the methodology for the design of an Interlaboratory Study (ILS) and calculation of precision estimates of a test method specified by the study. In particular, it defines the relevant statistical terms (Clause 3), the procedures to be adopted in the planning of ILS to determine the precision of a test method (Clause 4), and the method of calculating the precision from the results of such a study (Clauses 5 and 6).</p> <p>The procedures in ISO 4259-1:2017 have been designed specifically for petroleum and petroleum related products, which are normally considered as homogeneous. However, the procedures described in ISO 4259-1:2017 can also be applied to other types of homogeneous products. Careful investigations are necessary before applying ISO 4259-1:2017 to products for which the assumption of homogeneity can be questioned.</p>

Table of contents
View the extract
  • Avant-propos
  • 1 Domaine d'application
  • 2 Références normatives
  • 3 Termes et définitions
  • 4 Étapes de l'organisation d'un programme d'essai interlaboratoires pour la détermination de la fidélité d'une méthode d'essai
  • 5 Examen des résultats de l'essai interlaboratoires du point de vue de l'uniformité et des valeurs aberrantes
  • 6 Analyse de la variance, calcul et expression des estimations de fidélité
  • 7 Signification de la répétabilité ( r) et de la reproductibilité ( R)
  • 8 Spécifications
  • 9 Contrôle de qualité et spécifications
  • 10 Règles de conformité et de non-conformité, en cas de désaccord
  • Annexe A (normative) Détermination du nombre d'échantillons requis
  • Annexe C (normative) Notation et essais
  • Annexe D (normative) Exemples de résultats d'essais pour la détermination de l'indice de brome et tableaux statistiques
  • Annexe E (normative) Types de dépendance et transformations correspondantes
  • Annexe F (normative) Analyse de régression linéaire pondérée
  • Annexe G (normative) Règles d'arrondissage des résultats
  • Annexe B (informative) Établissement de l'équation de calcul du nombre d'échantillons requis
  • Annexe H (informative) Explication des équations données dans l'Article
    7
  • Annexe I (informative) Spécifications relatives à un degré spécifié de caractère critique
  • Bibliographie
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