NF ISO 1407

NF ISO 1407

March 2012
Standard Cancelled

Rubber - Determination of solvent extract

ISO 1407:2011 specifies four methods for the quantitative determination of the material extractable from raw rubbers, both natural and synthetic; two of the methods are also applicable to the unvulcanized and vulcanized compounds of raw rubbers. Method A measures the mass of the solvent extract, after evaporation of the solvent, relative to the mass of the original test portion. Method B measures the difference in the mass of the test portion before and after extraction. Method C, which is for raw rubbers only, measures the difference in the mass of the test portion before and after extraction using boiling solvent. Method D, which is for raw rubbers only, measures the difference in the mass of the test portion before and after extraction relative to the mass of the original test portion. Recommendations as to the solvent most appropriate for each type of rubber are given in an annex.

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Main informations

Collections

National standards and national normative documents

Publication date

March 2012

Number of pages

22 p.

Reference

NF ISO 1407

ICS Codes

83.040.10   Latex and raw rubber
83.060   Rubber

Classification index

T46-100

Print number

1 - 16/02/2012

International kinship

Sumary
Rubber - Determination of solvent extract

ISO 1407:2011 specifies four methods for the quantitative determination of the material extractable from raw rubbers, both natural and synthetic; two of the methods are also applicable to the unvulcanized and vulcanized compounds of raw rubbers.

Method A measures the mass of the solvent extract, after evaporation of the solvent, relative to the mass of the original test portion.

Method B measures the difference in the mass of the test portion before and after extraction.

Method C, which is for raw rubbers only, measures the difference in the mass of the test portion before and after extraction using boiling solvent.

Method D, which is for raw rubbers only, measures the difference in the mass of the test portion before and after extraction relative to the mass of the original test portion.

Recommendations as to the solvent most appropriate for each type of rubber are given in an annex.

Replaced standards (1)
NF ISO 1407
August 2010
Standard Cancelled
Rubber - Determination of solvent extract

Le présent document spécifie trois méthodes pour la détermination quantitative des matériaux pouvant être extraits des caoutchoucs bruts, naturels et synthétiques, et de leurs composés vulcanisés et non vulcanisés.

Standard replaced by (1)
NF ISO 1407
June 2023
Standard Current
Rubber - Determination of solvent extract

<p class="MsoBodyText"><span lang="EN-GB">This document specifies four methods for the quantitative determination of the material extractable from raw rubbers, both natural and synthetic; two of the methods are also applicable to the unvulcanized and vulcanized rubber compounds.</span></p> <p class="MsoBodyText"><span lang="EN-GB">Method A measures the mass of the solvent extract, after evaporation of the solvent, relative to the mass of the original test portion.</span></p> <p class="MsoBodyText"><span lang="EN-GB">Method B measures the difference in the mass of the test portion before and after extraction.</span></p> <p class="MsoBodyText"><span lang="EN-GB">Method C, which is for raw rubbers only, measures the difference in the mass of the test portion before and after extraction using boiling solvent.</span></p> <p class="MsoBodyText"><span lang="EN-GB">Method D, which is for raw rubbers only, measures the difference in the mass of the test portion before and after extraction relative to the mass of the original test portion.</span></p> <p class="Note"><span lang="EN-GB">NOTE 1<span style="mso-tab-count: 1;">        </span>Depending on the test method used, the conditioning of the test portion and the solvent used, the test result is not necessarily the same.</span></p> <p class="Note"><span lang="EN-GB">NOTE 2<span style="mso-tab-count: 1;">        </span>Method C generally gives results which are lower than those obtained with methods A and B due to an equilibrium which is set up, particularly if large test portions are used, depending on the content and the nature of the extractable matter. Method C is, however, a quicker method than method A or method B.</span></p> <p class="Note"><span lang="EN-GB">NOTE 3<span style="mso-tab-count: 1;">        </span>Methods C and D are not suitable if the test portion disintegrates during the extraction.</span></p> <p class="Note"><span lang="EN-GB">NOTE 4<span style="mso-tab-count: 1;">        </span>Method D is normally used for production controls.</span></p> <p class="MsoBodyText"><span lang="EN-GB">Recommendations as to the solvent most appropriate for each type of rubber are given in Annex A.</span></p>

Table of contents
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  • Avant-propos
    iv
  • 1 Domaine d'application
    1
  • 2 Références normatives
    1
  • 3 Principe
    2
  • 4 Solvant
    2
  • 5 Appareillage
    2
  • 6 Préparation des éprouvettes
    2
  • 6.1 Méthodes A et B
    2
  • 6.2 Méthode C (caoutchoucs bruts uniquement)
    2
  • 6.3 Méthode D (caoutchoucs bruts uniquement)
    4
  • 7 Mode opératoire
    4
  • 7.1 Généralités
    4
  • 7.2 Méthode A
    4
  • 7.3 Méthode B
    5
  • 7.4 Méthode C
    5
  • 7.5 Méthode D
    6
  • 8 Calcul et expression des résultats
    7
  • 8.1 Méthode A
    7
  • 8.2 Méthode B
    8
  • 8.3 Méthode C
    8
  • 8.4 Méthode D
    8
  • 8.5 Expression des résultats
    8
  • 9 Fidélité
    8
  • 10 Rapport d'essai
    8
  • Annexe A (informative) Solvants recommandés
    10
  • Annexe B (informative) Fidélité
    12
  • Annexe C (informative) Exemple de détermination du nombre minimal de cycles d'extraction pour une combinaison caoutchouc brut plus solvant d'EPDM et de 2-butanone
    16
  • Bibliographie
    18
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