NF ISO 14594

NF ISO 14594

June 2007
Standard Cancelled

Microbeam analysis - Electron probe microanalysis - Guidelines for the determination of experimental parameters for wavelength dispersive spectroscopy

ISO 14594:2003 gives the general guidelines for the determination of experimental parameters relating to the primary beam, the wavelength spectrometer and the sample that need to be taken into account when carrying out electron probe microanalysis. It also defines procedures for the determination of beam current, current density, dead time, wavelength resolution, background, analysis area, analysis depth and analysis volume. ISO 14594:2003 is intended for the analysis of a well-polished sample using normal beam incidence, and the parameters obtained may only be indicative for other experimental conditions.

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Main informations

Collections

National standards and national normative documents

Publication date

June 2007

Number of pages

22 p.

Reference

NF ISO 14594

ICS Codes

71.040.50   Physicochemical methods of analysis

Classification index

X21-002

Print number

2 - 01/03/2013

International kinship

Sumary
Microbeam analysis - Electron probe microanalysis - Guidelines for the determination of experimental parameters for wavelength dispersive spectroscopy

ISO 14594:2003 gives the general guidelines for the determination of experimental parameters relating to the primary beam, the wavelength spectrometer and the sample that need to be taken into account when carrying out electron probe microanalysis. It also defines procedures for the determination of beam current, current density, dead time, wavelength resolution, background, analysis area, analysis depth and analysis volume.

ISO 14594:2003 is intended for the analysis of a well-polished sample using normal beam incidence, and the parameters obtained may only be indicative for other experimental conditions.

Table of contents
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  • Avant-propos
    iv
  • 1 Domaine d'application
    1
  • 2 Références normatives
    1
  • 3 Termes et définitions
    1
  • 4 Abréviations
    2
  • 5 Paramètres expérimentaux
    2
  • 5.1 Généralités
    2
  • 5.2 Paramètres liés au faisceau primaire
    2
  • 5.3 Paramètres liés aux spectromètres à dispersion de longueur d'onde
    3
  • 5.4 Paramètres liés à l'échantillon
    5
  • 6 Modes opératoires et mesures
    5
  • 6.1 Généralités
    5
  • 6.2 Courant de faisceau
    5
  • 6.3 Paramètres liés aux pics mesurés
    6
  • 6.4 Paramètres liés à l'échantillon
    9
  • 7 Rapport d'essai
    9
  • Annexe A (informative) Méthodes d'estimation de l'aire d'analyse
    11
  • Annexe B (informative) Méthodes d'estimation de la profondeur d'analyse
    13
  • Annexe C (informative) Méthode d'estimation du volume analysé par simulation de Monte-Carlo (MC)
    14
  • Bibliographie
    18
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