NF ISO 4407

NF ISO 4407

September 2002
Standard Current

Hydraulic fluid power - Fluid contamination - Determination of particulate contamination by the counting method using an optical microscope

This International Standard specifies methods for determining the level of particulate contamination in liquids used in hydraulic systems by counting the number of particles deposited on the surface of a membrane filter using an optical microscope. It includes particle counting by two manual methods and image analysis, using either transmitted or incident lighting systems. Particle sizes greater than or equal to 2 micrometres can be sized and counted by this method, but the resolution and accuracy of the results will depend upon the optical system used and the capabilities of the operator. All hydraulic fluids with a wide range of contamination levels can be analysed according to this International Standard. However, the counting uncertainty at the larger particle sizes increases if the volume filtered is reduced to allow smaller sized particles to be counted, where a fine precipitate or a high particle concentration is present.

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Main informations

Collections

National standards and national normative documents

Publication date

September 2002

Number of pages

21 p.

Reference

NF ISO 4407

ICS Codes

23.100.60   Filters, seals and contamination of fluids
75.120   Hydraulic fluids

Classification index

E48-651

Print number

1 - 07/12/2002

International kinship

Sumary
Hydraulic fluid power - Fluid contamination - Determination of particulate contamination by the counting method using an optical microscope

This International Standard specifies methods for determining the level of particulate contamination in liquids used in hydraulic systems by counting the number of particles deposited on the surface of a membrane filter using an optical microscope. It includes particle counting by two manual methods and image analysis, using either transmitted or incident lighting systems.

Particle sizes greater than or equal to 2 micrometres can be sized and counted by this method, but the resolution and accuracy of the results will depend upon the optical system used and the capabilities of the operator.

All hydraulic fluids with a wide range of contamination levels can be analysed according to this International Standard. However, the counting uncertainty at the larger particle sizes increases if the volume filtered is reduced to allow smaller sized particles to be counted, where a fine precipitate or a high particle concentration is present.

Replaced standards (1)
NF E48-651
October 1986
Standard Cancelled
Hydraulic fluid power. Fluids. Determination of particulate contamination by the counting method using a microscope.

La présente norme fait partie d'un ensemble de normes françaises destinées à mesurer la pollution des fluides utilisés dans les transmissions hydrauliques. La méthode de comptage au microscope est importante car, bien que relativement longue et coûteuse, elle représente "la méthode de référence" permettant de juger les autres méthodes.

Table of contents
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  • Avant-propos
    iv
  • Introduction
    v
  • 1 Domaine d'application
    1
  • 2 Références normatives
    1
  • 3 Termes et définitions
    2
  • 4 Principe de comptage
    4
  • 5 Appareillage
    4
  • 6 Réactif et produits chimiques
    6
  • 6.1 Réactif et produits chimiques de rinçage et de nettoyage
    6
  • 6.2 Liquides de transparisation de la membrane filtrante (méthode en lumière transmise)
    6
  • 7 Mode opératoire de nettoyage de la verrerie
    7
  • 8 Méthodes d'étalonnage
    7
  • 8.1 Étalonnage du microscope
    7
  • 8.2 Détermination de la surface utile de filtration (SUF)
    7
  • 9 Préparation de la membrane filtrante
    8
  • 9.1 Préparation de l'échantillon
    8
  • 9.2 Analyse à blanc
    8
  • 9.3 Séparation des polluants par filtration sous vide
    9
  • 9.4 Évaluation de l'aptitude au comptage
    10
  • 9.5 Montage des membranes pour observation en lumière transmise
    10
  • 10 Classification des particules et méthode de comptage
    11
  • 10.1 Classification des particules
    11
  • 10.2 Choix du grossissement nominal
    11
  • 10.3 Méthode de comptage statistique
    11
  • 10.4 Calcul du nombre total
    12
  • 10.5 Vérification des résultats
    13
  • 11 Expression des résultats
    14
  • 12 Phrase d'identification (Référence à la présente Norme internationale)
    14
  • Bibliographie
    15
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