NF EN ISO 18857-1

NF EN ISO 18857-1

November 2006
Standard Current

Water quality - Determination of selected alkylphenols - Part 1 : method for non-filtered samples using liquid-liquid extraction and gas chromatography with mass selective detection

ISO 18857-1:2005 specifies a method for the determination of 4-nonylphenol (mixture of isomers) and 4-(1,1,3,3-tetramethylbutyl)phenol in non-filtered samples of drinking water, ground water and surface water. The method is applicable in a concentration range from 0,005 micrograms per litre to 0,2 micrograms per litre for 4-(1,1,3,3-tetramethylbutyl)phenol and from 0,02 micrograms per litre to 0,2 micrograms per litre for 4-nonylphenol (mixture of isomers). Depending on the matrix, the method is also applicable to waste water containing the analyzed compounds in the concentration range from 0,1 micrograms per litre to 50 micrograms per litre. Higher concentrations can be measured after appropriate dilution of the sample.

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Main informations

Collections

National standards and national normative documents

Publication date

November 2006

Number of pages

27 p.

Reference

NF EN ISO 18857-1

ICS Codes

13.060.50   Examination of water for chemical substances

Classification index

T90-184-1

Print number

1 - 10/10/2006

International kinship

European kinship

EN ISO 18857-1:2006
Sumary
Water quality - Determination of selected alkylphenols - Part 1 : method for non-filtered samples using liquid-liquid extraction and gas chromatography with mass selective detection

ISO 18857-1:2005 specifies a method for the determination of 4-nonylphenol (mixture of isomers) and 4-(1,1,3,3-tetramethylbutyl)phenol in non-filtered samples of drinking water, ground water and surface water. The method is applicable in a concentration range from 0,005 micrograms per litre to 0,2 micrograms per litre for 4-(1,1,3,3-tetramethylbutyl)phenol and from 0,02 micrograms per litre to 0,2 micrograms per litre for 4-nonylphenol (mixture of isomers). Depending on the matrix, the method is also applicable to waste water containing the analyzed compounds in the concentration range from 0,1 micrograms per litre to 50 micrograms per litre. Higher concentrations can be measured after appropriate dilution of the sample.

Table of contents
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  • Avant-propos
    iv
  • 1 Domaine d'application
    1
  • 2 Références normatives
    1
  • 3 Principe
    2
  • 4 Interférences
    2
  • 5 Réactifs
    2
  • 6 Appareillage
    3
  • 7 Prélèvement et prétraitement de l'échantillon
    4
  • 8 Mode opératoire
    4
  • 9 Étalonnage
    6
  • 10 Calcul
    11
  • 11 Expression des résultats
    12
  • 12 Rapport d'essai
    12
  • Annexe A (informative) Exemples de colonnes capillaires
    13
  • Annexe B (informative) Exemples de chromatogrammes
    14
  • Annexe C (informative) Essais de récupération - 4-nonylphénol (mélange d'isomères)
    16
  • Annexe D (informative) Exemple de séparateur
    17
  • Annexe E (informative) Données relatives à la performance de la méthode
    18
  • Bibliographie
    19
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