NF ISO 10382

NF ISO 10382

March 2003
Standard Cancelled

Soil quality - Determination of organochlorine pesticides and polychlorinated biphenyls - Gas-chromatographic method with electron capture detection

ISO 10382:2002 specifies a method for quantitative determination of seven polychlorinated biphenyls and seventeen organochlorine pesticides in soil. ISO 10382:2002 is applicable to all types of soil. Under the conditions specified in ISO 10382:2002, limits of detection of 0,1 micrograms per kilogram to 4 micrograms per kilogram (expressed as dry matter) can be achieved.

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Main informations

Collections

National standards and national normative documents

Publication date

March 2003

Number of pages

27 p.

Reference

NF ISO 10382

ICS Codes

13.080.10   Chemical characteristics of soils

Classification index

X31-118

Print number

1 - 06/03/2003

International kinship

ISO 10382:2002
Sumary
Soil quality - Determination of organochlorine pesticides and polychlorinated biphenyls - Gas-chromatographic method with electron capture detection

ISO 10382:2002 specifies a method for quantitative determination of seven polychlorinated biphenyls and seventeen organochlorine pesticides in soil.

ISO 10382:2002 is applicable to all types of soil.

Under the conditions specified in ISO 10382:2002, limits of detection of 0,1 micrograms per kilogram to 4 micrograms per kilogram (expressed as dry matter) can be achieved.

Table of contents
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  • Avant-propos
    iv
  • 1 Domaine d'application
    1
  • 2 Références normatives
    1
  • 3 Principe
    1
  • 4 Réactifs
    2
  • 5 Appareillage
    4
  • 6 Préparation des solutions étalons de PCB et de POC
    7
  • 7 Échantillonnage et conservation des échantillons
    8
  • 7.1 Échantillonnage
    8
  • 7.2 Conservation et prétraitement des échantillons
    8
  • 8 Mode opératoire
    8
  • 8.1 Essai à blanc
    8
  • 8.2 Extraction et concentration
    8
  • 8.3 Purification de l'extrait
    9
  • 8.4 Séparation par chromatographie en colonnes entre PCB et POC non polaires d'une part et plusieurs POC polaires d'autre part
    10
  • 8.5 Analyse par chromatographie en phase gazeuse
    10
  • 9 Rapport d'essai
    14
  • 10 Exactitude
    15
  • Annexe A (informative) Tableau des temps de rétention de biphényles polychlorés et de pesticides organochlorés pour deux colonnes capillaires différentes
    16
  • Annexe B (informative) Schéma de préparation de solutions étalons comprenant les étalons internes
    17
  • Annexe C (informative) Résultats d'un essai interlaboratoires réalisé aux Pays-Bas
    18
  • Annexe D (informative) Élimination du soufre élémentaire et de certains autres composés soufrés organiques
    21
  • Bibliographie
    23
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