NF ISO 12828-1
Validation method for fire gas analysis - Part 1 : limits of detection and quantification
In ISO 12828-1:2007, limits of detection and limits of quantification are defined and calculated. It provides methods for determining suitable values for these two parameters for a specific analytical procedure and for a specific chemical species. It does not provide detailed guidance on methods of sampling and analysis of specific species which might be present in fire effluents. This guidance is contained in ISO 19701 and ISO 19702.
In ISO 12828-1:2007, limits of detection and limits of quantification are defined and calculated. It provides methods for determining suitable values for these two parameters for a specific analytical procedure and for a specific chemical species. It does not provide detailed guidance on methods of sampling and analysis of specific species which might be present in fire effluents. This guidance is contained in ISO 19701 and ISO 19702.
- Avant-proposiv
- Introductionv
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1 Domaine d'application1
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2 Références normatives2
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3 Termes et définitions2
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4 Symboles3
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5 Remarques d'ordre général3
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5.1 Limite de détection: tableau des risques3
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5.2 Limite de quantification: effet sur la répétabilité, r3
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5.3 Valeurs généralement admises des limites de détection et de quantification4
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6 Méthodes de détermination des limites de détection et de quantification5
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6.1 Principes et aperçu des méthodes5
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6.2 Méthode principale 1 - Détermination de LD et LQ à partir des données d'une matrice issue d'échantillons à blanc6
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6.3 Méthode principale 2 - Détermination de LD et LQ à partir de la linéarité des données d'étalonnage8
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6.4 Méthode principale 3 - Vérification d'une limite de quantification donnée ou spécifiée10
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6.5 Autres méthodes11
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7 Expression des résultats12
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7.1 Exigences minimales12
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7.2 Expression des résultats d'analyse13
- Annexe A (informative) Exemples d'applications14
- Annexe B (informative) Exemples de l'importance des limites de détection et de quantification18
- Bibliographie21
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