NF ISO 20424

NF ISO 20424

June 2020
Standard Current

Fatty acid methyl esters (FAME) - Determination of sulfur content - Inductively coupled plasma optical emission spectrometry (ICP-OES) method

This document specifies a test method for inductively coupled plasma optical emission spectrometry (ICP-OES) for the detection of the sulfur content from 2 mg/kg to 21 mg/kg in fatty acid methyl esters (FAME). NOTE 1 For the purposes of this document, the term "% (m/m)" is used to represent the mass fraction (µ) of the material. NOTE 2 The method can also be used for the determination of concentrations outside the given limits. The precision statement, however, is only valid for the concentration range given in the scope. NOTE 3 The method described in the document was tested with FAME derived from soybean oil and beef tallow. FAME derived from other feedstock, in particular aged oils, may behave different due to the different nature of sulfur compounds.

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Main informations

Collections

National standards and national normative documents

Publication date

June 2020

Number of pages

16 p.

Reference

NF ISO 20424

ICS Codes

75.160.40   Biofuels

Classification index

M07-169

Print number

1

International kinship

Sumary
Fatty acid methyl esters (FAME) - Determination of sulfur content - Inductively coupled plasma optical emission spectrometry (ICP-OES) method

This document specifies a test method for inductively coupled plasma optical emission spectrometry (ICP-OES) for the detection of the sulfur content from 2 mg/kg to 21 mg/kg in fatty acid methyl esters (FAME).

NOTE 1 For the purposes of this document, the term "% (m/m)" is used to represent the mass fraction (µ) of the material.

NOTE 2 The method can also be used for the determination of concentrations outside the given limits. The precision statement, however, is only valid for the concentration range given in the scope.

NOTE 3 The method described in the document was tested with FAME derived from soybean oil and beef tallow. FAME derived from other feedstock, in particular aged oils, may behave different due to the different nature of sulfur compounds.

Table of contents
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  • 1 Domaine d'application
  • 2 Références normatives
  • 3 Termes et définitions
  • 4 Principe
  • 5 Produits et réactifs
  • 6 Appareillage
  • 7 Échantillonnage
  • 8 Préparation de la solution mère et des solutions d'étalonnage
  • 9 Étalonnage
  • 10 Mode opératoire
  • 11 Expression des résultats
  • 12 Contrôle qualité
  • 13 Fidélité
  • 14 Rapport d'essai
  • Annexe A Calcul de la concentration d'une huile de faible viscosité dans une solution de blanc
  • Annexe B Étude interlaboratoires - Échantillons d'EMAG utilisés pour établir les valeurs de fidélité
  • Bibliographie
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