NF ISO 6145-9

NF ISO 6145-9

December 2009
Standard Cancelled

Gas analysis - Preparation of calibration gas mixtures using dynamic volumetric methods - Part 9 : saturation method

ISO 6145-9:2009 is one of a series of International Standards dealing with various dynamic volumetric methods used for the preparation of calibration gas mixtures. This part specifies a method for continuous production of calibration gas mixtures containing one or more readily condensable components. A relative expanded uncertainty of measurement, U, obtained by multiplying the relative combined standard uncertainty by a coverage factor k = 2, of not greater than ±1 %, can be obtained using this method. Unlike the methods presented in the other parts of ISO 6145, the method described in this part does not require accurate measurement of flow rates since flow rates do not appear in the equations for calculation of the volume fraction. Readily condensable gases and vapours commonly become adsorbed on surfaces, and it is therefore difficult to prepare stable calibration gas mixtures of accurately known composition, containing such components, by means of static methods. In addition, these calibration gas mixtures cannot be maintained under a pressure near the saturation limit without the occurrence of condensation. The saturation method can be employed to prepare mixtures of this type.

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Main informations

Collections

National standards and national normative documents

Publication date

December 2009

Number of pages

20 p.

Reference

NF ISO 6145-9

ICS Codes

71.040.40   Chemical analysis

Classification index

X20-205-9

Print number

1 - 16/12/2009

International kinship

Sumary
Gas analysis - Preparation of calibration gas mixtures using dynamic volumetric methods - Part 9 : saturation method

ISO 6145-9:2009 is one of a series of International Standards dealing with various dynamic volumetric methods used for the preparation of calibration gas mixtures. This part specifies a method for continuous production of calibration gas mixtures containing one or more readily condensable components. A relative expanded uncertainty of measurement, U, obtained by multiplying the relative combined standard uncertainty by a coverage factor k = 2, of not greater than ±1 %, can be obtained using this method.

Unlike the methods presented in the other parts of ISO 6145, the method described in this part does not require accurate measurement of flow rates since flow rates do not appear in the equations for calculation of the volume fraction.

Readily condensable gases and vapours commonly become adsorbed on surfaces, and it is therefore difficult to prepare stable calibration gas mixtures of accurately known composition, containing such components, by means of static methods. In addition, these calibration gas mixtures cannot be maintained under a pressure near the saturation limit without the occurrence of condensation. The saturation method can be employed to prepare mixtures of this type.

Standard replaced by (1)
NF EN ISO 6145-9
April 2011
Standard Current
Gas analysis - Preparation of calibration gas mixtures using dynamic volumetric methods - Part 9 : saturation method

<p>ISO 6145-9:2009 is one of a series of International Standards dealing with various dynamic volumetric methods used for the preparation of calibration gas mixtures. This part specifies a method for continuous production of calibration gas mixtures containing one or more readily condensable components. A relative expanded uncertainty of measurement, <i>U</i>, obtained by multiplying the relative combined standard uncertainty by a coverage factor <i>k</i> = 2, of not greater than ±1 %, can be obtained using this method.</p> <p>Unlike the methods presented in the other parts of ISO 6145, the method described in this part does not require accurate measurement of flow rates since flow rates do not appear in the equations for calculation of the volume fraction.</p> <p>Readily condensable gases and vapours commonly become adsorbed on surfaces, and it is therefore difficult to prepare stable calibration gas mixtures of accurately known composition, containing such components, by means of static methods. In addition, these calibration gas mixtures cannot be maintained under a pressure near the saturation limit without the occurrence of condensation. The saturation method can be employed to prepare mixtures of this type.</p>

Table of contents
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  • Avant-propos
    iv
  • 1 Domaine d'application
    1
  • 2 Références normatives
    1
  • 3 Termes et définitions
    1
  • 4 Principe
    2
  • 5 Appareillage
    2
  • 5.1 Montage
    2
  • 5.2 Préparation du gaz
    2
  • 5.3 Compatibilité de l'appareillage
    2
  • 5.4 Choix de l'appareillage
    2
  • 5.5 Contrôle de la pression
    3
  • 5.6 Contrôle de la température
    3
  • 5.7 Instruments
    4
  • 5.8 Pureté
    4
  • 6 Mode opératoire
    4
  • 6.1 Installation
    4
  • 6.2 Fonctionnement du système direct
    4
  • 6.3 Fonctionnement du système de circulation fermé
    4
  • 7 Incertitude de mesure
    5
  • Annexe A (normative) Vue d'ensemble des données relatives à la tension de vapeur pour diverses substances
    7
  • Annexe B (informative) Exemples d'estimations de l'incertitude
    11
  • Bibliographie
    14
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