XP ISO/TS 28037

XP ISO/TS 28037

August 2013
Standard Current

Détermination and use of straight-line calibration functions

ISO/TS 28037:2010 is concerned with linear, that is, straight-line, calibration functions that describe the relationship between two variables X and Y, namely, functions of the form Y = A + BX. Although many of the principles apply to more general types of calibration function, the approaches described exploit the simple form of the straight-line calibration function wherever possible. Values of the parameters A and B are determined on the basis of measured data points (xi, yi), i = 1, ... , m. Various cases are considered relating to the nature of the uncertainties associated with these data. No assumption is made that the errors relating to the yi are homoscedastic (having equal variance), and similarly for the xi when the errors are not negligible. Estimates of the parameters A and B are determined using least squares methods. The emphasis is on choosing the least squares method most appropriate for the type of measurement data, in particular methods that reflect the associated uncertainties. The most general type of covariance matrix associated with the measurement data is treated, but important special cases that lead to simpler calculations are described in detail. For all cases considered, methods for validating the use of the straight-line calibration functions and for evaluating the uncertainties and covariance associated with the parameter estimates are given. ISO/TS 28037:2010 also describes the use of the calibration function parameter estimates and their associated uncertainties and covariance to predict a value of X and its associated standard uncertainty given a measured value of Y and its associated standard uncertainty.

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Main informations

Collections

National standards and national normative documents

Publication date

August 2013

Number of pages

55 p.

Reference

XP ISO/TS 28037

ICS Codes

03.120.30   Application of statistical methods

Classification index

X06-077

Print number

1 - 23/08/2013

International kinship

Sumary
Détermination and use of straight-line calibration functions

ISO/TS 28037:2010 is concerned with linear, that is, straight-line, calibration functions that describe the relationship between two variables X and Y, namely, functions of the form Y = A + BX. Although many of the principles apply to more general types of calibration function, the approaches described exploit the simple form of the straight-line calibration function wherever possible.

Values of the parameters A and B are determined on the basis of measured data points (xi, yi), i = 1, ... , m. Various cases are considered relating to the nature of the uncertainties associated with these data. No assumption is made that the errors relating to the yi are homoscedastic (having equal variance), and similarly for the xi when the errors are not negligible.

Estimates of the parameters A and B are determined using least squares methods. The emphasis is on choosing the least squares method most appropriate for the type of measurement data, in particular methods that reflect the associated uncertainties. The most general type of covariance matrix associated with the measurement data is treated, but important special cases that lead to simpler calculations are described in detail.

For all cases considered, methods for validating the use of the straight-line calibration functions and for evaluating the uncertainties and covariance associated with the parameter estimates are given.

ISO/TS 28037:2010 also describes the use of the calibration function parameter estimates and their associated uncertainties and covariance to predict a value of X and its associated standard uncertainty given a measured value of Y and its associated standard uncertainty.

Table of contents
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  • Avant-propos
    v
  • Introduction
    vi
  • 1 Domaine d'application
    1
  • 2 Références normatives
    1
  • 3 Termes et définitions
    1
  • 4 Conventions et notation
    4
  • 5 Principes de l'étalonnage linéaire
    5
  • 5.1 Généralités
    5
  • 5.2 Éléments d'entrée pour la détermination de la fonction d'étalonnage
    5
  • 5.3 Détermination de la fonction d'étalonnage
    6
  • 5.4 Traitement numérique
    7
  • 5.5 Incertitudes et covariances associées aux paramètres de la fonction d'étalonnage
    7
  • 5.6 Validation du modèle
    8
  • 5.7 Utilisation de la fonction d'étalonnage
    8
  • 5.8 Détermination de la droite de meilleur ajustement des données par la méthode des moindres carrés ordinaires
    9
  • 6 Modèle applicable aux incertitudes associées à yi
    9
  • 6.1 Généralités
    9
  • 6.2 Estimations des paramètres d'étalonnage, des incertitudes-types et de la covariance associées
    10
  • 6.3 Validation du modèle
    11
  • 6.4 Organisation des calculs
    12
  • 7 Modèle applicable aux incertitudes associées à xi et yi
    16
  • 7.1 Généralités
    16
  • 7.2 Estimations des paramètres d'étalonnage, des incertitudes-types et de la covariance associées
    18
  • 7.3 Validation du modèle
    19
  • 7.4 Organisation des calculs
    20
  • 8 Modèle applicable aux incertitudes associées à xi et yi et aux covariances associées aux paires (xi, yi)
    24
  • 8.1 Généralités
    24
  • 8.2 Estimations des paramètres d'étalonnage et incertitudes-types et covariance associées.
    25
  • 9 Modèle applicable aux incertitudes et aux covariances associées à yi
    25
  • 9.1 Généralités
    25
  • 9.2 Estimations des paramètres d'étalonnage, incertitudes-types et covariance associées
    26
  • 9.3 Validation du modèle
    28
  • 9.4 Organisation des calculs
    28
  • 10 Modèle applicable aux incertitudes et aux covariances associées à xi et yi
    32
  • 10.1 Généralités
    32
  • 10.2 Estimations des paramètres d'étalonnage, des incertitudes-types et covariances associées
    33
  • 10.3 Validation du modèle
    35
  • 11 Utilisation de la fonction d'étalonnage
    39
  • 11.1 Prédiction directe
    39
  • 11.2 Prédiction inverse
    40
  • Annexe A (informative) Opérations matricielles
    42
  • Annexe B (informative) Application de l'algorithme de Gauss-Newton à la régression selon le critère de distance généralisée
    48
  • Annexe C (informative) Approche de factorisation orthogonale pour résoudre le problème de Gauss-Markov généralisé
    50
  • Annexe D (informative) Disposition relative aux incertitudes et covariances associées aux valeurs mesurées x et y
    56
  • Annexe E (informative) Incertitudes connues avec un facteur d'échelle donné
    61
  • Annexe F (informative) Application logicielle des algorithmes décrits
    66
  • Annexe G (informative) Glossaire des principaux symboles
    68
  • Bibliographie
    70
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