NF ISO 15202-2

NF ISO 15202-2

October 2020
Standard Current

Workplace air - Determination of metals and metalloids in airborne particulate matter by inductively coupled plasma atomic emission spectrometry - Part 2 : sample preparation

This document specifies a number of suitable methods for preparing test solutions from samples of airborne particulate matter collected using the method specified in ISO 15202?1, for subsequent determination of metals and metalloids by ICP?AES using the method specified in ISO 15202?3. It contains information about the applicability of the methods with respect to the measurement of metals and metalloids for which limit values have been set. The methods can also be used in the measurement of some metals and metalloids for which limit values have not been set but no information about its applicability is provided in this case.NOTE The sample preparation methods described in this document are generally suitable for use with analytical techniques other than ICP?AES, e.g. atomic absorption spectrometry (AAS) by ISO 8518[5] and ISO 11174[10] and inductively coupled plasma mass spectrometry (ICP?MS) by ISO 30011[11].The method specified in Annex B is applicable when making measurements for comparison with limit values for soluble metal or metalloid compounds.One or more of the sample dissolution methods specified in Annexes C through H are applicable when making measurements for comparison with limit values for total metals and metalloids and their compounds. Information on the applicability of individual methods is given in the scope of the annex in which the method is specified.The following is a non-exclusive list of metals and metalloids for which limit values have been set (see References [14] and [15]) and for which one or more of the sample dissolution methods specified in this document are applicable. However, there is no information available on the effectiveness of any of the specified sample dissolution methods for those elements in italics.AluminiumCalciumMagnesiumSeleniumTungstenAntimonyChromiumManganeseSilverUraniumArsenicCobaltMercurySodiumVanadiumBariumCopperMolybdenumStrontiumYttriumBerylliumHafniumNickelTantalumZincBismuthIndiumPhosphorusTelluriumZirconiumBoronIronPlatinumThalliumCaesiumLeadPotassiumTinCadmiumLithiumRhodiumTitaniumISO 15202 is not applicable to the determination of elemental mercury or arsenic trioxide, since mercury vapour and arsenic trioxide vapour are not collected using the sampling method specified in ISO 15202?1.

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Main informations

Collections

National standards and national normative documents

Thematics

Gestion des risques et SST

Publication date

October 2020

Number of pages

55 p.

Reference

NF ISO 15202-2

ICS Codes

13.040.30   Workplace atmospheres

Classification index

X43-265-2

Print number

1

International kinship

ISO 15202-2:2002:2020
Sumary
Workplace air - Determination of metals and metalloids in airborne particulate matter by inductively coupled plasma atomic emission spectrometry - Part 2 : sample preparation

This document specifies a number of suitable methods for preparing test solutions from samples of airborne particulate matter collected using the method specified in ISO 15202?1, for subsequent determination of metals and metalloids by ICP?AES using the method specified in ISO 15202?3. It contains information about the applicability of the methods with respect to the measurement of metals and metalloids for which limit values have been set. The methods can also be used in the measurement of some metals and metalloids for which limit values have not been set but no information about its applicability is provided in this case.

NOTE The sample preparation methods described in this document are generally suitable for use with analytical techniques other than ICP?AES, e.g. atomic absorption spectrometry (AAS) by ISO 8518[5] and ISO 11174[10] and inductively coupled plasma mass spectrometry (ICP?MS) by ISO 30011[11].

The method specified in Annex B is applicable when making measurements for comparison with limit values for soluble metal or metalloid compounds.

One or more of the sample dissolution methods specified in Annexes C through H are applicable when making measurements for comparison with limit values for total metals and metalloids and their compounds. Information on the applicability of individual methods is given in the scope of the annex in which the method is specified.

The following is a non-exclusive list of metals and metalloids for which limit values have been set (see References [14] and [15]) and for which one or more of the sample dissolution methods specified in this document are applicable. However, there is no information available on the effectiveness of any of the specified sample dissolution methods for those elements in italics.

Aluminium

Calcium

Magnesium

Selenium

Tungsten

Antimony

Chromium

Manganese

Silver

Uranium

Arsenic

Cobalt

Mercury

Sodium

Vanadium

Barium

Copper

Molybdenum

Strontium

Yttrium

Beryllium

Hafnium

Nickel

Tantalum

Zinc

Bismuth

Indium

Phosphorus

Tellurium

Zirconium

Boron

Iron

Platinum

Thallium

Caesium

Lead

Potassium

Tin

Cadmium

Lithium

Rhodium

Titanium

ISO 15202 is not applicable to the determination of elemental mercury or arsenic trioxide, since mercury vapour and arsenic trioxide vapour are not collected using the sampling method specified in ISO 15202?1.

Replaced standards (1)
NF ISO 15202-2
March 2012
Standard Cancelled
Workplace air - Determination of metals and metalloids in airborne particulate matter by inductively coupled plasma atomic emission spectrometry - Part 2 : sample preparation

1.1 This part of ISO 15202 specifies a number of suitable methods for preparing test solutions from samples of airborne particulate matter collected using the method specified in ISO 15202‑1, for subsequent determination of metals and metalloids by ICP‑AES using the method specified in ISO 15202‑3. It contains information about the applicability of the methods with respect to the measurement of metals and metalloids for which limit values have been set. The methods can also be used in the measurement of some metals and metalloids for which limit values have not been set but no information about its applicability is provided in this case. NOTE The sample preparation methods described in this part of ISO 15202 are generally suitable for use with analytical techniques other than ICP‑AES, e.g. atomic absorption spectrometry (AAS) by ISO 8518[5] and ISO 11174[10] and inductively coupled plasma mass spectrometry (ICP‑MS) by ISO 30011[11]. 1.2 The method specified in Annex B is applicable when making measurements for comparison with limit values for soluble metal or metalloid compounds. 1.3 One or more of the sample dissolution methods specified in Annexes C through H are applicable when making measurements for comparison with limit values for total metals and metalloids and their compounds. Information on the applicability of individual methods is given in the scope of the annex in which the method is specified. 1.4 The following is a non-exclusive list of metals and metalloids for which limit values have been set (see References [15] and [16]) and for which one or more of the sample dissolution methods specified in this part of ISO 15202 are applicable. However, there is no information available on the effectiveness of any of the specified sample dissolution methods for those elements in italics. Aluminium Calcium Magnesium Selenium Tungsten Antimony Chromium Manganese Silver Uranium Arsenic Cobalt Mercury Sodium Vanadium Barium Copper Molybdenum Strontium Yttrium Beryllium Hafnium Nickel Tantalum Zinc Bismuth Indium Phosphorus Tellurium Zirconium Boron Iron Platinum Thallium Caesium Lead Potassium Tin Cadmium Lithium Rhodium Titanium ISO 15202 is not applicable to the determination of elemental mercury or arsenic trioxide, since mercury vapour and arsenic trioxide vapour are not collected using the sampling method specified in ISO 15202‑1.

Table of contents
  • 1 Domaine d'application
  • 2 Références normatives
  • 3 Termes et définitions
  • 4 Principe
  • 5 Exigences
  • 6 Réactions
  • 7 Réactifs
  • 8 Appareillage de laboratoire
  • 9 Mode opératoire
  • 10 Cas particuliers
  • 11 Enregistrements de laboratoire
  • Annexe A Précautions de sécurité à respecter lors de l'utilisation d'acide fluorhydrique et perchlorique
  • Annexe B Méthode de mise en solution d'échantillon pour les composés solubles de métaux et métalloïdes
  • Annexe C Mise en solution d'échantillon à l'aide d'acide nitrique et d'acide chlorhydrique sur plaque chauffante
  • Annexe D Mise en solution d'échantillon à l'aide d'acide fluorhydrique et d'acide nitrique par agitation par ultrason
  • Annexe E Mise en solution en utilisant de l'acide sulfurique et du peroxyde d'hydrogène sur plaque chauffante
  • Annexe F Mise en solution en utilisant de l'acide nitrique et de l'acide perchlorique sur plaque chauffante
  • Annexe G Mise en solution d'échantillon dans un système de digestion par micro-ondes en récipient fermé
  • Annexe H Mise en solution d'échantillon à 95 °C sur bloc chauffant
  • Annexe I Action à mener en présence de particules visibles, non dissoutes, après mise en solution d'échantillon
  • Annexe J Dépôts sur les parois des dispositifs de prélèvement
  • Bibliographie
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