NF ISO 30011

December 2010

Standard Current

Workplace air - Determination of metals and metalloids in airborne particulate matter by inductively coupled plasma mass spectrometry

ISO 30011:2010 specifies a procedure for the use of quadrupole inductively coupled plasma mass spectrometry (ICP‑MS) for analysing test solutions prepared from samples of airborne particulate matter collected as specified in ISO 15202‑1. Method development, performance checks, and a routine analysis method are specified. Test solutions for analysis by ISO 30011:2010 are prepared as specified in ISO 15202‑2. ISO 30011:2010 is applicable to the assessment of workplace exposure to metals and metalloids for comparison with limit values.

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Main informations

Collections

National standards and national normative documents

Thematics

Gestion des risques et SST

Publication date

December 2010

Number of pages

43 p.

Reference

NF ISO 30011

ICS Codes

13.040.30 Workplace atmospheres

Classification index

X43-207

Print number

1 - 13/12/2010

International kinship

ISO 30011:2010

Sumary

Workplace air - Determination of metals and metalloids in airborne particulate matter by inductively coupled plasma mass spectrometry

Test solutions for analysis by ISO 30011:2010 are prepared as specified in ISO 15202‑2.

ISO 30011:2010 is applicable to the assessment of workplace exposure to metals and metalloids for comparison with limit values.

Table of contents

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Avant-propos
iv
Introduction
v
1 Domaine d'application
1
2 Références normatives
2
3 Termes et définitions
2
3.1 Définitions générales
2
3.2 Définitions relatives à l'analyse
3
3.3 Définitions relatives à l'ICP-MS
6
3.4 Définitions relatives aux statistiques
8
4 Principe
10
5 Exigences
10
6 Réactifs
10
7 Appareillage
13
8 Mode opératoire
14
8.1 Préparation des solutions d'échantillon
14
8.2 Développement de la méthode
14
8.3 Vérifications des performances de l'instrument
19
8.4 Analyse de routine
20
8.5 Estimation des limites de détection et de quantification
21
8.6 Contrôle de la qualité
22
8.7 Incertitude de mesure
23
9 Expression des résultats
23
10 Performances de la méthode
24
10.1 Limites de détection et de quantification de la méthode
24
10.2 Limites supérieures de la gamme d'analyse
25
10.3 Biais et fidélité
25
10.4 Incertitude de mesure
25
11 Rapport d'essai
26
11.1 Procès-verbal de l'essai
26
11.2 Rapport de laboratoire
27
Annexe A (informative) Principes de l'ICP-MS et interférences
28
Annexe B (informative) Recommandations relatives à la maintenance des instruments d'ICP-MS
31
Annexe C (informative) Nouveau calcul des concentrations de métaux et de métalloïdes dans l'air pour les conditions de référence
34
Bibliographie
35

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