FD ISO/TS 21748
Guidance for the use of repeatability, reproductibility and trueness estimates in measurement uncertainty estimation
TS 21748:2004 gives guidance for the evaluation of measurement uncertainties using data obtained from studies conducted in accordance with ISO 5725-2, and for the comparison of collaborative study results with measurement uncertainty obtained using formal principles of uncertainty propagation. TS 21748:2003 is applicable in all measurement and test fields where an uncertainty associated with a result has to be determined, but does not describe the application of repeatability data in the absence of reproducibility data. The recommendations in this document are primarily for guidance.
TS 21748:2004 gives guidance for the evaluation of measurement uncertainties using data obtained from studies conducted in accordance with ISO 5725-2, and for the comparison of collaborative study results with measurement uncertainty obtained using formal principles of uncertainty propagation. TS 21748:2003 is applicable in all measurement and test fields where an uncertainty associated with a result has to be determined, but does not describe the application of repeatability data in the absence of reproducibility data. The recommendations in this document are primarily for guidance.
ISO 21748:2010 gives guidance for evaluation of measurement uncertainties using data obtained from studies conducted in accordance with ISO 5725-2:1994; comparison of collaborative study results with measurement uncertainty (MU) obtained using formal principles of uncertainty propagation. (ISO 5725-3:1994 provides additional models for studies of intermediate precision. However, while the same general approach may be applied to the use of such extended models, uncertainty evaluation using these models is not incorporated in ISO 21748:2010.) ISO 21748:2010 is applicable in all measurement and test fields where an uncertainty associated with a result has to be determined. It does not describe the application of repeatability data in the absence of reproducibility data. ISO 21748:2010 assumes that recognized, non-negligible systematic effects are corrected, either by applying a numerical correction as part of the method of measurement, or by investigation and removal of the cause of the effect. The recommendations in ISO 21748:2010 are primarily for guidance. It is recognized that while the recommendations presented do form a valid approach to the evaluation of uncertainty for many purposes, it is also possible to adopt other suitable approaches. In general, references to measurement results, methods and processes in ISO 21748:2010 are normally understood to apply also to testing results, methods and processes.
- Avant-proposiv
- Introductionv
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1 Domaine d'application1
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2 Références normatives1
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3 Termes et définitions2
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4 Symboles4
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5 Principes7
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5.1 Résultats individuels et performance du processus de mesure7
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5.2 Utilisation des données de reproductibilité7
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5.3 Équations fondamentales pour le modèle statistique7
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5.4 Données de répétabilité8
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6 Évaluation de l'incertitude de mesure à l'aide des estimations de la répétabilité, de la reproductibilité et de la justesse9
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6.1 Procédure pour l'évaluation de l'incertitude de mesure9
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6.2 Différences entre fidélité attendue et fidélité réelle9
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7 Établissement de la pertinence des données de performance de la méthode aux résultats de mesure à partir d'un processus de mesure particulier9
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7.1 Généralités9
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7.2 Démonstration du contrôle du composant de biais du laboratoire9
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7.3 Vérification de la répétabilité12
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7.4 Vérification continue de la performance12
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8 Établissement de la pertinence de l'individu d'essai13
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8.1 Généralités13
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8.2 Échantillonnage13
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8.3 Préparation et traitement préalable des échantillons13
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8.4 Changements du type d'individu d'essai13
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8.5 Variation de l'incertitude avec le niveau de réponse14
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9 Facteurs supplémentaires14
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10 Expression générale pour l'estimation de l'incertitude-type composée15
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11 Budgets d'incertitude fondés sur des données d'études collaboratives15
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12 Évaluation de l'incertitude pour un résultat composé17
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13 Expression des données d'incertitude17
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13.1 Expression générale17
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13.2 Choix du facteur d'élargissement17
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14 Comparaison des valeurs de performance d'une méthode et des données d'incertitude18
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14.1 Hypothèses de base18
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14.2 Procédure d'essai18
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14.3 Raisons des différences19
- Annexe A (informative) Méthodes d'estimation de l'incertitude20
- Annexe B (informative) Évaluation expérimentale de l'incertitude25
- Annexe C (informative) Exemples de calcul de l'incertitude de mesure26
- Bibliographie31
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