NF EN ISO 11357-1

NF EN ISO 11357-1

December 2009
Standard Cancelled

Plastics - Differential scanning calorimetry (DSC) - Part 1 : general principles

ISO 11357 specifies several differential scanning calorimetry (DSC) methods for the thermal analysis of polymers and polymer blends, such asthermoplastics (polymers, moulding compounds and other moulding materials, with or without fillers, fibres or reinforcements);thermosets (uncured or cured materials, with or without fillers, fibres or reinforcements);elastomers (with or without fillers, fibres or reinforcements).ISO 11357 is intended for the observation and measurement of various properties of the above-mentioned materials, such asphysical transitions (glass transition, phase transitions such as melting and crystallization, polymorphic transitions, etc.);chemical reactions (polymerization, crosslinking and curing of elastomers and thermosets, etc.);the stability to oxidation;the heat capacity.ISO 11357-1:2009 specifies a number of general aspects of differential scanning calorimetry, such as the principle and the apparatus, sampling, calibration and general aspects of the procedure and test report common to all following parts.Details on performing specific methods are given in subsequent parts of ISO 11357.

See more
View the extract
Main informations

Collections

National standards and national normative documents

Publication date

December 2009

Number of pages

42 p.

Reference

NF EN ISO 11357-1

ICS Codes

83.080.01   Plastics in general

Classification index

T51-507-1

Print number

1 - 08/12/2009

International kinship

ISO 11357-1:2009

European kinship

EN ISO 11357-1:2009
Sumary
Plastics - Differential scanning calorimetry (DSC) - Part 1 : general principles

ISO 11357 specifies several differential scanning calorimetry (DSC) methods for the thermal analysis of polymers and polymer blends, such as

  • thermoplastics (polymers, moulding compounds and other moulding materials, with or without fillers, fibres or reinforcements);
  • thermosets (uncured or cured materials, with or without fillers, fibres or reinforcements);
  • elastomers (with or without fillers, fibres or reinforcements).

ISO 11357 is intended for the observation and measurement of various properties of the above-mentioned materials, such as

  • physical transitions (glass transition, phase transitions such as melting and crystallization, polymorphic transitions, etc.);
  • chemical reactions (polymerization, crosslinking and curing of elastomers and thermosets, etc.);
  • the stability to oxidation;
  • the heat capacity.

ISO 11357-1:2009 specifies a number of general aspects of differential scanning calorimetry, such as the principle and the apparatus, sampling, calibration and general aspects of the procedure and test report common to all following parts.

Details on performing specific methods are given in subsequent parts of ISO 11357.

Replaced standards (1)
NF EN ISO 11357-1
July 1997
Standard Cancelled
Plastics. Differential scanning calorimetry (DSC). Part 1 : general principles.

Standard replaced by (1)
NF EN ISO 11357-1
December 2016
Standard Cancelled
Plastics - Differential scanning calorimetry (DSC) - Part 1 : general principles

ISO 11357-1:2016 specifies several differential scanning calorimetry (DSC) methods for the thermal analysis of polymers and polymer blends, such as - thermoplastics (polymers, moulding compounds and other moulding materials, with or without fillers, fibres or reinforcements), - thermosets (uncured or cured materials, with or without fillers, fibres or reinforcements), and - elastomers (with or without fillers, fibres or reinforcements). ISO 11357-1:2016 is intended for the observation and measurement of various properties of, and phenomena associated with, the above-mentioned materials, such as - physical transitions (glass transition, phase transitions such as melting and crystallization, polymorphic transitions, etc.), - chemical reactions (polymerization, crosslinking and curing of elastomers and thermosets, etc.), - the stability to oxidation, and - the heat capacity. ISO 11357-1:2016 specifies a number of general aspects of differential scanning calorimetry, such as the principle and the apparatus, sampling, calibration and general aspects of the procedure and test report common to all following parts. Details on performing specific methods are given in subsequent parts of ISO 11357 (see Foreword).

Table of contents
  • Avant-propos
    IV
  • Introduction
    VI
  • 1 Domaine d'application
    1
  • 2 Références normatives
    2
  • 3 Termes et définitions
    2
  • 4 Principe
    8
  • 4.1 Généralités
    8
  • 4.2 DSC à flux thermique
    8
  • 4.3 DSC à compensation de puissance
    8
  • 5 Appareillage et matériaux
    9
  • 6 Éprouvettes
    10
  • 7 Conditions d'essai et conditionnement des éprouvettes
    11
  • 7.1 Conditions d'essai
    11
  • 7.2 Conditionnement des éprouvettes
    11
  • 8 Étalonnage
    11
  • 8.1 Généralités
    11
  • 8.2 Matériaux d'étalonnage
    12
  • 8.3 Étalonnage en température
    12
  • 8.4 Étalonnage en chaleur
    14
  • 8.5 Étalonnage en flux thermique
    15
  • 9 Mode opératoire
    17
  • 9.1 Mise en service de l'appareillage
    17
  • 9.2 Chargement de l'éprouvette dans le creuset
    18
  • 9.3 Mise en place des creusets dans l'appareil
    19
  • 9.4 Réalisation des mesurages
    19
  • 9.5 Vérification après mesurages
    21
  • 10 Rapport d'essai
    21
  • Annexe A (normative) Étalonnage en température de haute précision, étendu (11)
    23
  • Annexe B (normative) Étalonnage en chaleur de haute précision, étendu
    25
  • Annexe C (informative) Matériaux étalons recommandés
    27
  • Annexe D (informative) Interaction entre les matériaux d'étalons et les différents matériaux des creusets
    30
  • Annexe E (informative) Recommandations générales
    32
  • Bibliographie
    34
Need to identify, monitor and decipher standards?

COBAZ is the simple and effective solution to meet the normative needs related to your activity, in France and abroad.

Available by subscription, CObaz is THE modular solution to compose according to your needs today and tomorrow. Quickly discover CObaz!

Request your free, no-obligation live demo

I discover COBAZ