NF EN ISO 14577-4

NF EN ISO 14577-4

August 2007
Standard Cancelled

Metallic materials - Instrumented indentation test for hardness and materials parameters - Part 4 : test method for metallic and non-metallic coatings

ISO 14577-4:2007 specifies a method for testing coatings that is particularly suitable for testing in the nano/micro range applicable to thin coatings.This test method is limited to the examination of single layers when the indentation is carried out normal to the test piece surface, but graded and multilayer coatings can also be measured in cross-section if the thickness of the individual layers or gradations is greater than the spatial resolution of the indentation process.The test method is not limited to any particular type of material. Metallic, non-metallic and organic coatings are included in the scope of ISO 14577-4:2007.The application of ISO 14577-4:2007 regarding measurement of hardness is only possible if the indenter is a pyramid or a cone with a radius of tip curvature small enough for plastic deformation to occur within the coating. The hardness of visco-elastic materials, or materials exhibiting significant creep will be strongly affected by the time taken to perform the test.

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Main informations

Collections

National standards and national normative documents

Publication date

August 2007

Number of pages

33 p.

Reference

NF EN ISO 14577-4

ICS Codes

77.040.10   Mechanical testing of metals

Classification index

A03-155-4

Print number

1 - 07/08/2007

International kinship

European kinship

EN ISO 14577-4:2007
Sumary
Metallic materials - Instrumented indentation test for hardness and materials parameters - Part 4 : test method for metallic and non-metallic coatings

ISO 14577-4:2007 specifies a method for testing coatings that is particularly suitable for testing in the nano/micro range applicable to thin coatings.

This test method is limited to the examination of single layers when the indentation is carried out normal to the test piece surface, but graded and multilayer coatings can also be measured in cross-section if the thickness of the individual layers or gradations is greater than the spatial resolution of the indentation process.

The test method is not limited to any particular type of material. Metallic, non-metallic and organic coatings are included in the scope of ISO 14577-4:2007.

The application of ISO 14577-4:2007 regarding measurement of hardness is only possible if the indenter is a pyramid or a cone with a radius of tip curvature small enough for plastic deformation to occur within the coating. The hardness of visco-elastic materials, or materials exhibiting significant creep will be strongly affected by the time taken to perform the test.

Standard replaced by (1)
NF EN ISO 14577-4
April 2017
Standard Current
Metallic materials - Instrumented indentation test for hardness and materials parameters - Part 4 : test method for metallic and non-metallic coatings

ISO 14577-4:2016 specifies a method for testing coatings which is particularly suitable for testing in the nano/micro range applicable to thin coatings. However, the application of this method of this part of ISO 14577 is not needed if the indentation depth is such a small fraction of the coating thickness that in any possible case a substrate influence can be neglected and the coating can be considered as a bulk material. Limits for such cases are given. This test method is limited to the examination of single layers when the indentation is carried out normal to the test piece surface, but graded and multilayer coatings can also be measured in cross-section if the thickness of the individual layers or gradations is greater than the spatial resolution of the indentation process. The test method is not limited to any particular type of material. Metallic and non-metallic coatings are included in the scope of this part of ISO 14577. In this part of ISO 14577, the term coating is used to refer to any solid layer with homogeneous properties different to that of a substrate it is connected to. The method assumes that coating properties are constant with indentation depth. Composite coatings are considered to be homogenous if the structure size is less than the indentation size. The application of this part of ISO 14577 regarding measurement of indentation hardness is only possible if the indenter is a pyramid or a cone with a radius of tip curvature small enough for plastic deformation to occur within the coating. The hardness of visco-elastic materials or materials exhibiting significant creep will be strongly affected by the time taken to perform the test.

Table of contents
  • Avant-propos
    iv
  • Introduction
    v
  • 1 Domaine d'application
    1
  • 2 Références normatives
    1
  • 3 Symboles et désignations
    2
  • 4 Vérification et étalonnage des machines d'essai
    3
  • 5 Éprouvettes
    3
  • 5.1 Généralités
    3
  • 5.2 Rugosité de surface
    5
  • 5.3 Polissage
    5
  • 5.4 Propreté de surface
    6
  • 5.5 Exgences particulières pour les peintures et vernis
    6
  • 6 Mode opératoire
    6
  • 6.1 Conditions d'essai
    6
  • 6.2 Mode opératoire de mesure
    9
  • 7 Analyse de données et évaluation des résultats pour des pénétrations perpendiculairement à la surface
    12
  • 7.1 Généralités
    12
  • 7.2 Module de pénétration du revêtement
    13
  • 7.3 Dureté de pénétration du revêtement
    14
  • 8 Rapport d'essai
    17
  • Annexe A (normative) Procédure d'étalonnage de la complaisance du bâti
    18
  • Annexe B (normative) Point de contact et régime purement élastique
    22
  • Bibliographie
    24
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