NF EN ISO 19581

NF EN ISO 19581

February 2020
Standard Current

Measurement of radioactivity - Gamma emitting radionuclides - Rapid screening method using scintillation detector gamma-ray spectrometry

ISO 19581 specifies a screening test method to quantify rapidly the activity concentration of gamma-emitting radionuclides, such as 131I, 132Te, 134Cs and 137Cs, in solid or liquid test samples using gamma-ray spectrometry with lower resolution scintillation detectors as compared with the HPGe detectors (see IEC 61563). This test method can be used for the measurement of any potentially contaminated environmental matrices (including soil), food and feed samples as well as industrial materials or products that have been properly conditioned. Sample preparation techniques used in the screening method are not specified in ISO 19581, since special sample preparation techniques other than simple machining (cutting, grinding, etc.) should not be required. Although the sampling procedure is of utmost importance in the case of the measurement of radioactivity in samples, it is out of scope of ISO 19581; other international standards for sampling procedures that can be used in combination with ISO 19581 are available (see References [1],[2],[3],[4],[5],[6]). The test method applies to the measurement of gamma-emitting radionuclides such as 131I, 134Cs and 137Cs. Using sample sizes of 0,5 l to 1,0 l in a Marinelli beaker and a counting time of 5 min to 20 min, decision threshold of 10 Bq·kg−1 can be achievable using a commercially available scintillation spectrometer [e.g. thallium activated sodium iodine (NaI(Tl)) spectrometer 2" ϕ × 2" detector size, 7 % resolution (FWHM) at 662 keV, 30 mm lead shield thickness]. This test method also can be performed in a "makeshift" laboratory or even outside a testing laboratory on samples directly measured in the field where they were collected. During a nuclear or radiological emergency, this test method enables a rapid measurement of the sample activity concentration of potentially contaminated samples to check against operational intervention levels (OILs) set up by decision makers that would trigger a predetermined emergency response to reduce existing radiation risks[12]. Due to the uncertainty associated with the results obtained with this test method, test samples requiring more accurate test results can be measured using high-purity germanium (HPGe) detectors gamma-ray spectrometry in a testing laboratory, following appropriate preparation of the test samples[7][8]. ISO 19581 does not contain criteria to establish the activity concentration of OILs.

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Main informations

Collections

National standards and national normative documents

Publication date

February 2020

Number of pages

28 p.

Reference

NF EN ISO 19581

ICS Codes

17.240   Radiation measurements

Classification index

M60-833

Print number

1

International kinship

European kinship

EN ISO 19581:2020
Sumary
Measurement of radioactivity - Gamma emitting radionuclides - Rapid screening method using scintillation detector gamma-ray spectrometry

ISO 19581 specifies a screening test method to quantify rapidly the activity concentration of gamma-emitting radionuclides, such as 131I, 132Te, 134Cs and 137Cs, in solid or liquid test samples using gamma-ray spectrometry with lower resolution scintillation detectors as compared with the HPGe detectors (see IEC 61563).

This test method can be used for the measurement of any potentially contaminated environmental matrices (including soil), food and feed samples as well as industrial materials or products that have been properly conditioned. Sample preparation techniques used in the screening method are not specified in ISO 19581, since special sample preparation techniques other than simple machining (cutting, grinding, etc.) should not be required. Although the sampling procedure is of utmost importance in the case of the measurement of radioactivity in samples, it is out of scope of ISO 19581; other international standards for sampling procedures that can be used in combination with ISO 19581 are available (see References [1],[2],[3],[4],[5],[6]).

The test method applies to the measurement of gamma-emitting radionuclides such as 131I, 134Cs and 137Cs. Using sample sizes of 0,5 l to 1,0 l in a Marinelli beaker and a counting time of 5 min to 20 min, decision threshold of 10 Bq·kg−1 can be achievable using a commercially available scintillation spectrometer [e.g. thallium activated sodium iodine (NaI(Tl)) spectrometer 2" ϕ × 2" detector size, 7 % resolution (FWHM) at 662 keV, 30 mm lead shield thickness].

This test method also can be performed in a "makeshift" laboratory or even outside a testing laboratory on samples directly measured in the field where they were collected.

During a nuclear or radiological emergency, this test method enables a rapid measurement of the sample activity concentration of potentially contaminated samples to check against operational intervention levels (OILs) set up by decision makers that would trigger a predetermined emergency response to reduce existing radiation risks[12].

Due to the uncertainty associated with the results obtained with this test method, test samples requiring more accurate test results can be measured using high-purity germanium (HPGe) detectors gamma-ray spectrometry in a testing laboratory, following appropriate preparation of the test samples[7][8].

ISO 19581 does not contain criteria to establish the activity concentration of OILs.

Replaced standards (1)
NF ISO 19581
July 2019
Standard Cancelled
Measurement of radioactivity - Gamma emitting radionuclides - Rapid screening method using scintillation detector gamma-ray spectrometry

<p>ISO 19581 specifies a screening test method to quantify rapidly the activity concentration of gamma-emitting radionuclides, such as <sup>131</sup>I, <sup>132</sup>Te, <sup>134</sup>Cs and <sup>137</sup>Cs, in solid or liquid test samples using gamma-ray spectrometry with lower resolution scintillation detectors as compared with the HPGe detectors (see IEC 61563).</p> <p>This test method can be used for the measurement of any potentially contaminated environmental matrices (including soil), food and feed samples as well as industrial materials or products that have been properly conditioned. Sample preparation techniques used in the screening method are not specified in ISO 19581, since special sample preparation techniques other than simple machining (cutting, grinding, etc.) should not be required. Although the sampling procedure is of utmost importance in the case of the measurement of radioactivity in samples, it is out of scope of ISO 19581; other international standards for sampling procedures that can be used in combination with ISO 19581 are available (see References [1],[2],[3],[4],[5],[6]).</p> <p>The test method applies to the measurement of gamma-emitting radionuclides such as <sup>131</sup>I, <sup>134</sup>Cs and <sup>137</sup>Cs. Using sample sizes of 0,5 l to 1,0 l in a Marinelli beaker and a counting time of 5 min to 20 min, decision threshold of 10 Bq·kg<sup>−1</sup> can be achievable using a commercially available scintillation spectrometer [e.g. thallium activated sodium iodine (NaI(Tl)) spectrometer 2" <i>ϕ</i> × 2" detector size, 7 % resolution (FWHM) at 662 keV, 30 mm lead shield thickness].</p> <p>This test method also can be performed in a "makeshift" laboratory or even outside a testing laboratory on samples directly measured in the field where they were collected.</p> <p>During a nuclear or radiological emergency, this test method enables a rapid measurement of the sample activity concentration of potentially contaminated samples to check against operational intervention levels (OILs) set up by decision makers that would trigger a predetermined emergency response to reduce existing radiation risks<sup>[12]</sup>.</p> <p>Due to the uncertainty associated with the results obtained with this test method, test samples requiring more accurate test results can be measured using high-purity germanium (HPGe) detectors gamma-ray spectrometry in a testing laboratory, following appropriate preparation of the test samples<sup>[7][8]</sup>.</p> <p>ISO 19581 does not contain criteria to establish the activity concentration of OILs.</p>

Table of contents
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  • 1 Domaine d'application
  • 2 Références normatives
  • 3 Termes et définitions
  • 4 Symboles et unités
  • 5 Principe
  • 6 Appareillage
  • 7 Récipient à échantillon
  • 8 Mode opératoire
  • 9 Rapport d'essai
  • Annexe A Exemple d'application de l'ISO 19581 pour la présélection du radiocésium
  • Bibliographie
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