NF EN ISO 307
Plastics - Polyamides - Determination of viscosity number
This document specifies a method for the determination of the viscosity number of dilute solutions of polyamides in certain specified solvents.The method is applicable to the polyamides designated PA 46, PA 6, PA 66, PA 69, PA 610, PA 612, PA 11, PA 12, PA 6T/66, PA 6I/6T, PA 6T/6I/66, PA 6T/6I, PA 6I/6T/66 and PA MXD6 as defined in ISO 16396-1, as well as to copolyamides, compounds of polyamides and other polyamides that are soluble in one of the specified solvents under the specified conditions.The method is not applicable to polyamides produced by anionic polymerization of lactams or produced with cross-linking agents; such polyamides are normally insoluble in the specified solvents.The viscosity number is determined by the general procedure specified in ISO 1628?1, observing the particular conditions specified in this document.
This document specifies a method for the determination of the viscosity number of dilute solutions of polyamides in certain specified solvents.
The method is applicable to the polyamides designated PA 46, PA 6, PA 66, PA 69, PA 610, PA 612, PA 11, PA 12, PA 6T/66, PA 6I/6T, PA 6T/6I/66, PA 6T/6I, PA 6I/6T/66 and PA MXD6 as defined in ISO 16396-1, as well as to copolyamides, compounds of polyamides and other polyamides that are soluble in one of the specified solvents under the specified conditions.
The method is not applicable to polyamides produced by anionic polymerization of lactams or produced with cross-linking agents; such polyamides are normally insoluble in the specified solvents.
The viscosity number is determined by the general procedure specified in ISO 1628?1, observing the particular conditions specified in this document.
ISO 307:2007 specifies a method for the determination of the viscosity number of dilute solutions of polyamides in certain specified solvents. For pure polyamides or polyamides containing additives that do not interfere with the viscosity measurement, the determination of the viscosity number of a polyamide provides a measure of the molecular mass of the polymer. The viscosity number of pure polyamides or polyamides which contain additives that do not interfere with the viscosity measurement can be converted from one solvent to another. The viscosity number of polyamides containing additives that do interfere with the viscosity measurement is specific to the solvent used and the material composition. In this case, the measured viscosity number cannot be converted from one solvent to another. The method is applicable to the polyamides designated PA 46, PA 6, PA 66, PA 69, PA 610, PA 612, PA 11, PA 12, PA 6T/66, PA 6I/6T, PA 6T/6I/66, PA 6T/6I, PA 6I/6T/66 and PA MXD6, as well as to copolyamides, compounds of polyamides and other polyamides that are soluble in one of the specified solvents under the specified conditions. The method is not applicable to polyamides produced by anionic polymerization of lactams or produced with cross-linking agents; such polyamides are normally insoluble in the specified solvents.
Le présent document apporte des modifications techniques et éditoriales à la norme NF EN ISO 307 de décembre 2007.
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1 Domaine d'application
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2 Références normatives
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3 Termes et définitions
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4 Principe
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5 Réactifs et matériaux
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6 Appareillage
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7 Préparation des échantillons pour essai
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8 Calcul de la masse de la prise d'essai
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9 Choix du solvant
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10 Mode opératoire
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11 Expression des résultats
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12 Répétabilité et reproductibilité
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13 Relation entre l'indice de viscosité déterminé dans une solution d'acide sulfurique à 96 pour cent (fraction massique) et la viscosité relative déterminée dans différents autres solvants
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14 Rapport d'essai
- Annexe A Détermination de la concentration de l'acide sulfurique commercial (95 pour cent à 98 pour cent ) et ajustement à 96 pour cent par titrage
- Annexe B Détermination de la concentration de l'acide sulfurique (95 pour cent à 98 pour cent ) et ajustement à 96 pour cent par mesurage du temps d'écoulement dans un petit viscosimètre capillaire
- Annexe C Détermination de la concentration de l'acide formique commercial et ajustement à 90 pour cent par titrage
- Annexe D Détermination de la concentration de l'acide formique commercial à 90 pour cent par mesurage de la masse volumique
- Annexe E Relation entre l'indice de viscosité déterminé dans une solution d'acide sulfurique à 96 pour cent (fraction massique) et la viscosité déterminée dans différents solvants
- Bibliographie
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