NF ISO 12830
Paper, board and pulps - Determination of acid-soluble magnesium, calcium, manganese, iron, copper, sodium and potassium
ISO 12830:2011 specifies the procedure for the determination of acid-soluble magnesium, calcium, manganese, iron, copper, sodium and potassium by atomic absorption spectrometry or by plasma emission spectrometry. The acid-soluble element comprises the acid-soluble part of the incineration residue, i.e. that part of the ignition residue obtained after incineration which is soluble in hydrochloric acid. In the case where the residue is completely soluble, the result obtained by the procedure specified in this International Standard is a measure of the total amount of each element in the sample. ISO 12830:2011 is applicable to all types of paper, board and pulps. The limit of determination depends on the element and on the instrument used.
ISO 12830:2011 specifies the procedure for the determination of acid-soluble magnesium, calcium, manganese, iron, copper, sodium and potassium by atomic absorption spectrometry or by plasma emission spectrometry. The acid-soluble element comprises the acid-soluble part of the incineration residue, i.e. that part of the ignition residue obtained after incineration which is soluble in hydrochloric acid. In the case where the residue is completely soluble, the result obtained by the procedure specified in this International Standard is a measure of the total amount of each element in the sample.
ISO 12830:2011 is applicable to all types of paper, board and pulps.
The limit of determination depends on the element and on the instrument used.
<p>This document specifies the procedure for the determination of acid-soluble magnesium, calcium, manganese, iron, copper, sodium and potassium by atomic absorption spectrometry (AAS) or by inductively coupled plasma emission spectrometry (ICP/ES). The acid-soluble element comprises the acid-soluble part of the incineration residue, i.e. that part of the ignition residue obtained after incineration which is soluble in hydrochloric acid or nitric acid. In cases where the residue is completely soluble, the result obtained by the procedure specified in this document is a measure of the total amount of each element in the sample.</p> <p>This document is applicable to all types of paper, board, pulps and cellulose nanomaterials.</p> <p>The limit of determination depends on the element and on the instrument used.</p>
- Avant-proposiv
- Introductionv
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1 Domaine d'application1
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2 Références normatives1
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3 Principe1
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4 Réactifs et matériaux1
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5 Appareillage et équipement3
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6 Échantillonnage et préparation de l'échantillon3
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7 Mode opératoire3
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7.1 Généralités3
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7.2 Incinération de la prise d'essai4
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7.3 Dissolution du résidu4
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8 Préparation des solutions d'étalonnage4
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8.1 Spectrométrie d'absorption atomique (AAS)4
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8.2 Spectrométrie d'émission plasma (ICP/ES)5
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9 Solution à blanc5
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10 Détermination5
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11 Calculs6
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12 Rapport d'essai6
- Annexe A (informative) Fidélité7
- Bibliographie12
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