NF ISO 15009

NF ISO 15009

February 2003
Standard Cancelled

Soil quality - Gas chromatographic determination of the content of volatile aromatic hydrocarbons, naphthalene and volatile halogenated hydrocarbons - Purge and trap method with thermal desorption

ISO 15009:2002 specifies a method for quantitative gas-chromatographic determination of volatile hydrocarbons, naphthalene and volatile halogenated hydrocarbons in soil.ISO 15009:2002 is applicable to all types of soil.Under the conditions specified in ISO 15009:2002, the following limits of determinations apply (expressed on basis of dry matter):volatile hydrocarbons and naphthalene: 0,1 mg/kg;volatile halogenated hydrocarbons: 0,01 mg/kg.The lower limit of determination is dependent on the equipment used and the quality of the methanol grade used for the extraction of the soil sample.

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National standards and national normative documents

Publication date

February 2003

Number of pages

22 p.

Reference

NF ISO 15009

ICS Codes

13.080.10   Chemical characteristics of soils

Classification index

X31-426

Print number

1 - 06/03/2003

International kinship

ISO 15009:2002
Sumary
Soil quality - Gas chromatographic determination of the content of volatile aromatic hydrocarbons, naphthalene and volatile halogenated hydrocarbons - Purge and trap method with thermal desorption

ISO 15009:2002 specifies a method for quantitative gas-chromatographic determination of volatile hydrocarbons, naphthalene and volatile halogenated hydrocarbons in soil.

ISO 15009:2002 is applicable to all types of soil.

Under the conditions specified in ISO 15009:2002, the following limits of determinations apply (expressed on basis of dry matter):

  • volatile hydrocarbons and naphthalene: 0,1 mg/kg;
  • volatile halogenated hydrocarbons: 0,01 mg/kg.

The lower limit of determination is dependent on the equipment used and the quality of the methanol grade used for the extraction of the soil sample.

Standard replaced by (1)
NF ISO 15009
September 2012
Standard Cancelled
Soil quality - Gas chromatographic determination of the content of volatile aromatic hydrocarbons, naphthalene and volatile halogenated hydrocarbons - Purge-and-trap method with thermal desorption

Ce document spécifie une méthode pour la détermination quantitative par chromatographie en phase gazeuse des hydrocarbures volatils, du naphtalène et des hydrocarbures halogénés volatils contenus dans les sols. Il est applicable à tous les types de sols. La limite inférieure de détermination dépend du matériel utilisé et de la qualité du méthanol utilisé pour l'extraction de l'échantillon de sol. Dans les conditions spécifiées dans la présente Norme internationale, les limites de dosage suivantes (exprimées par rapport à la matière sèche) s'appliquent : hydrocarbures aromatiques volatils : 0,1 mg/kg ; hydrocarbures halogénés volatils : 0,01 mg/kg. Des limites de dosage plus faibles peuvent être atteintes pour certains composés si l'on utilise la spectrométrie de masse (SM) avec détection sélective des ions.

Table of contents
  • Avant-propos
    iv
  • 1
    Domaine d'application 1
  • 2
    Références normatives 1
  • 3
    Principe 2
  • 4
    Réactifs 2
  • 5
    Préparation des solutions étalon 4
  • 6
    Appareillage 5
  • 7
    Échantillonnage, conservation et prétraitement de l'échantillon 8
  • 8
    Mode opératoire 8
  • 8.1
    Détermination à blanc 8
  • 8.2
    Teneur en matière sèche 8
  • 8.3
    Extraction 8
  • 8.4
    Purge et piégeage 8
  • 8.5
    Analyse par chromatographie en phase gazeuse 9
  • 9
    Calcul 10
  • 9.1
    Principe 10
  • 9.2
    Mode opératoire 11
  • 10
    Expression des résultats 12
  • 11
    Fidélité 12
  • 12
    Rapport d'essai 12
  • Annexe A (informative) Temps de rétention relatifs pour l'éthylbenzène-D10 des hydrocarbures aromatiques volatils et des hydrocarbures halogénés volatils sur les colonnes CP-Sil 5 CB et CP-Sil 13 CB
    13
  • Annexe B (informative) Validation
    15
  • Bibliographie
    18
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