NF ISO 16000-4
Indoor air - Part4 : determination of formaldehyde - Diffusive sampling method
ISO 16000-4:2011 specifies a determination of formaldehyde in indoor air using a diffusive sampler with solvent desorption and high performance liquid chromatography (HPLC).The test method is applicable to the measurement of formaldehyde in indoor air over the range from 0,001 mg/m3 to 1,0 mg/m3 for a sampling period of between 24 h and 72 h. For sampling periods of 24 h, the applicable concentration range is 0,003 mg/m3 to 1 mg/m3, and for 72 h it is 0,001 mg/m3 to 0,33 mg/m3.The method is suitable for measurements in atmospheres with conventional indoor air relative humidity and for monitoring at air velocities as low as 0,02 m/s. The chromatographic step in the method is designed to eliminate potential interferences, including those due to the presence of other carbonyl compounds. The sampling method gives a time-weighted average result.
ISO 16000-4:2011 specifies a determination of formaldehyde in indoor air using a diffusive sampler with solvent desorption and high performance liquid chromatography (HPLC).
The test method is applicable to the measurement of formaldehyde in indoor air over the range from 0,001 mg/m3 to 1,0 mg/m3 for a sampling period of between 24 h and 72 h. For sampling periods of 24 h, the applicable concentration range is 0,003 mg/m3 to 1 mg/m3, and for 72 h it is 0,001 mg/m3 to 0,33 mg/m3.
The method is suitable for measurements in atmospheres with conventional indoor air relative humidity and for monitoring at air velocities as low as 0,02 m/s. The chromatographic step in the method is designed to eliminate potential interferences, including those due to the presence of other carbonyl compounds. The sampling method gives a time-weighted average result.
Le présent document décrit une méthode par échantillonnage diffisif/désorption de solvant/chromatographie en phase liquide à haute performance (HPLC) pour le dosage du formaldéhyde dans l'air intérieur. La méthode d'essai s'applique au mesurage du formaldéhyde dans l'air intérieur sur la gamme comprise entre 0,001 mg/m3 et 1,0 mg/m3 pour une période d'échantillonnage comprise entre 24 h et 72 h. La méthode convient à des mesurages réalisés dans des atmosphères contenant jusqu'à 80 % d'humidité relative et à des vitesses d'air de l'ordre de 0,02 m/s.
- Avant-proposiv
- IntroductionVI
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1 Domaine d'application1
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2 Références normatives1
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3 Principe2
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4 Réactifs2
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5 Appareillage4
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6 Échantillonnage4
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7 Mode opératoire5
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7.1 Désorption et préparation de l'échantillon5
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7.2 Étalonnage5
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7.3 Analyse par CLHP5
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7.4 Détermination de la concentration de l'échantillon7
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7.5 Stockage7
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7.6 Détermination de l'efficacité de désorption7
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8 Calculs7
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8.1 Masse de DNPH-formaldéhyde sur le filtre7
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8.2 Concentration du formaldéhyde dans l'air7
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9 Fidélité et incertitude de la méthode8
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10 Assurance qualité/contrôle qualité8
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11 Rapport d'essai9
- Annexe A (informative) Conceptions types d'échantillonneurs par diffusion10
- Bibliographie12
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