NF ISO 18363-1

NF ISO 18363-1

December 2015
Standard Cancelled

Animal and vegetable fats and oils - Determination of fatty-acid-bound chloropropanediols (MCPDs) and glycidol by GC/MS - Part 1 : method using fast alkaline transesterification and measurement for 3-MCPD and differential measurement for glycidol

ISO 18363-1:2015 describes a procedure for the indirect determination of 3-MCPD esters (bound 3-MCPD) and possible free 3-MCPD after alkaline catalysed ester cleavage and derivatization with phenylboronic acid (PBA). Furthermore, this part of ISO 18363 enables the indirect determination of glycidyl esters (bound glycidol) under the assumption that no other substances are present that react at room temperature with inorganic chloride to generate 3-MCPD. ISO 18363-1:2015 is applicable to solid and liquid fats and oils. Milk and milk products (or fat coming from milk and milk products) are excluded from the scope of this part of ISO 18363.

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Main informations

Collections

National standards and national normative documents

Publication date

December 2015

Number of pages

17 p.

Reference

NF ISO 18363-1

ICS Codes

67.200.10   Animal and vegetable fats and oils

Classification index

T60-285-1

Print number

1

International kinship

Sumary
Animal and vegetable fats and oils - Determination of fatty-acid-bound chloropropanediols (MCPDs) and glycidol by GC/MS - Part 1 : method using fast alkaline transesterification and measurement for 3-MCPD and differential measurement for glycidol

ISO 18363-1:2015 describes a procedure for the indirect determination of 3-MCPD esters (bound 3-MCPD) and possible free 3-MCPD after alkaline catalysed ester cleavage and derivatization with phenylboronic acid (PBA). Furthermore, this part of ISO 18363 enables the indirect determination of glycidyl esters (bound glycidol) under the assumption that no other substances are present that react at room temperature with inorganic chloride to generate 3-MCPD.

ISO 18363-1:2015 is applicable to solid and liquid fats and oils. Milk and milk products (or fat coming from milk and milk products) are excluded from the scope of this part of ISO 18363.

Standard replaced by (1)
NF EN ISO 18363-1
December 2021
Standard Current
Animal and vegetable fats and oils - Determination of fatty-acid-bound chloropropanediols (MCPDs) and glycidol by GC/MS - Part 1 : method using fast alkaline transesterification and measurement for 3-MCPD and differential measurement for glycidol

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