NF ISO 18589-4

NF ISO 18589-4

May 2009
Standard Cancelled

Measurements of radioactivity in the environment - Soil - Part 4 : measurement of plutonium isotopes (plutonium 238 and plutonium 239 + 240) by alpha spectrometry

ISO 18589-4:2009 describes a method for measuring plutonium 238 and 239 + 240 isotopes in soil by alpha spectrometry samples using chemical separation techniques. The method can be used for any type of environmental study or monitoring. These techniques can also be used for measurements of very low levels of activity, one or two orders of magnitude less than the level of natural alpha-emitting radionuclides.The mass of the test portion required depends on the assumed activity of the sample and the desired detection limit. In practice, it can range from 0,1 g to 100 g of the test sample.

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Main informations

Collections

National standards and national normative documents

Thematics

Sécurité, Gestion des risques et SST, QSE

Publication date

May 2009

Number of pages

30 p.

Reference

NF ISO 18589-4

ICS Codes

13.280   Radiation protection
17.240   Radiation measurements
27.120.01   Nuclear energy in general

Classification index

M60-790-4

Print number

1 - 20/05/2009

International kinship

ISO 18589-4:2009
Sumary
Measurements of radioactivity in the environment - Soil - Part 4 : measurement of plutonium isotopes (plutonium 238 and plutonium 239 + 240) by alpha spectrometry

ISO 18589-4:2009 describes a method for measuring plutonium 238 and 239 + 240 isotopes in soil by alpha spectrometry samples using chemical separation techniques. The method can be used for any type of environmental study or monitoring. These techniques can also be used for measurements of very low levels of activity, one or two orders of magnitude less than the level of natural alpha-emitting radionuclides.

The mass of the test portion required depends on the assumed activity of the sample and the desired detection limit. In practice, it can range from 0,1 g to 100 g of the test sample.

Replaced standards (1)
NF M60-790-8
July 1999
Standard Cancelled
Nuclear energy. Measurement of radioactivity in the environment-Soil. Part 8 : methodology for plutonium 238 and plutonium 239 plus 240 activity measurement in soil samples.

Le présent document expose les principes de la mesure des isotopes 238 et 239 + 240 du plutonium dans les échantillons de sol et propose en annexe deux méthodes de séparation et de purification spécifiques.

Standard replaced by (1)
NF ISO 18589-4
August 2020
Standard Cancelled
Measurement of radioactivity in the environment - Soil - Part 4 : plutonium 238 and plutonium 239 + 240 - Test method using alpha spectrometry

This document describes a method for measuring 238Pu and 239 + 240 isotopes in soil by alpha spectrometry samples using chemical separation techniques. The method can be used for any type of environmental study or monitoring. These techniques can also be used for measurements of very low levels of activity, one or two orders of magnitude less than the level of natural alpha-emitting radionuclides. The test methods described in this document can also be used to measure the radionuclides in sludge, sediment, construction material and products following proper sampling procedure[2][3][4][5][7][8]. The mass of the test portion required depends on the assumed activity of the sample and the desired detection limit. In practice, it can range from 0,1 g to 100 g of the test sample.

Table of contents
  • Avant-propos
    iv
  • Introduction
    v
  • 1 Domaine d'application
    1
  • 2 Références normatives
    1
  • 3 Termes, définitions et symboles
    1
  • 4 Principe
    2
  • 5 Réactifs et appareillage
    2
  • 6 Mode opératoire
    3
  • 7 Expression des résultats
    4
  • 8 Rapport d'essai
    6
  • Annexe A (informative) Plutonium désorbé
    7
  • Annexe B (informative) Séparation chimique du plutonium par un solvant organique
    11
  • Annexe C (informative) Séparation chimique du plutonium sur une résine anionique
    13
  • Annexe D (informative) Séparation chimique du plutonium par des résines spécifiques
    15
  • Annexe E (informative) Préparation de la source par électrodéposition
    18
  • Annexe F (informative) Préparation de la source par coprécipitation
    21
  • Bibliographie
    22
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