NF ISO 22155

NF ISO 22155

January 2006
Standard Cancelled

Soil quality - Gas chromatographic quantitative determination of volatile aromatic and halogenated hydrocarbons and selected ethers - Static headspace method

ISO 22155:2005 specifies a static headspace method for quantitative gas chromatographic determination of volatile aromatic and halogenated hydrocarbons and selected aliphatic ethers in soil.ISO 22155:2005 is applicable to all types of soil.The limit of determination is dependent on the detection system used and the quality of the methanol grade used for the extraction of the soil sample.Under the conditions specified in ISO 22155:2005, the following limits of determinations apply (expressed on the basis of dry matter):when using gas chromatography with a flame ionization detector (GC-FID), the typical limit of determination is 0,2 mg/kg for volatile aromatic hydrocarbons, and 0,5 mg/kg for aliphatic ethers as methyl tert-butyl ether (MTBE) and tert-amyl methyl ether (TAME);when using gas chromatography with an electron capture detector (GC-ECD), the typical limit of determination is 0,01 mg/kg to 0,2 mg/kg for volatile halogenated hydrocarbons. Lower limits of determination can be achieved by using mass spectrometry (MS) with selected ion detection.

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Main informations

Collections

National standards and national normative documents

Publication date

January 2006

Number of pages

21 p.

Reference

NF ISO 22155

ICS Codes

13.080.10   Chemical characteristics of soils

Classification index

X31-438

Print number

1 - 23/12/2005

International kinship

ISO 22155:2005
Sumary
Soil quality - Gas chromatographic quantitative determination of volatile aromatic and halogenated hydrocarbons and selected ethers - Static headspace method

ISO 22155:2005 specifies a static headspace method for quantitative gas chromatographic determination of volatile aromatic and halogenated hydrocarbons and selected aliphatic ethers in soil.

ISO 22155:2005 is applicable to all types of soil.

The limit of determination is dependent on the detection system used and the quality of the methanol grade used for the extraction of the soil sample.

Under the conditions specified in ISO 22155:2005, the following limits of determinations apply (expressed on the basis of dry matter):

  1. when using gas chromatography with a flame ionization detector (GC-FID), the typical limit of determination is 0,2 mg/kg for volatile aromatic hydrocarbons, and 0,5 mg/kg for aliphatic ethers as methyl tert-butyl ether (MTBE) and tert-amyl methyl ether (TAME);
  2. when using gas chromatography with an electron capture detector (GC-ECD), the typical limit of determination is 0,01 mg/kg to 0,2 mg/kg for volatile halogenated hydrocarbons.

Lower limits of determination can be achieved by using mass spectrometry (MS) with selected ion detection.

Standard replaced by (1)
NF ISO 22155
May 2011
Standard Cancelled
Soil quality - Gas chromatographic determination of volatile aromatic and halogenated hydrocarbons and selected ethers - Static headspace method

ISO 22155:2011 specifies a static headspace method for quantitative gas chromatographic determination of volatile aromatic and halogenated hydrocarbons and selected aliphatic ethers in soil. ISO 22155:2011 is applicable to all types of soil. The limit of determination is dependent on the detection system used and the quality of the methanol grade used for the extraction of the soil sample. Under the conditions specified in ISO 22155:2011, the following limits of determination apply (expressed on the basis of dry matter): Typical limit of determination when using gas chromatography/flame ionization detection (GC/FID): volatile aromatic hydrocarbons: 0,2 mg/kg; aliphatic ethers as methyl tert-butyl ether (MTBE) and tert-amyl methyl ether (TAME): 0,5 mg/kg. Typical limit of determination when using gas chromatography/electron capture detection (GC/ECD): volatile halogenated hydrocarbons: 0,01 mg/kg to 0,2 mg/kg. Lower limits of determination can be achieved for some compounds by using mass spectrometry (MS) with selected ion detection.

Table of contents
  • Avant-propos
    iv
  • 1 Domaine d'application
    1
  • 2 Références normatives
    1
  • 3 Principe
    2
  • 4 Réactifs
    2
  • 5 Appareillage
    5
  • 6 Échantillonnage, conservation et traitement préliminaire des échantillons
    6
  • 7 Mode opératoire
    7
  • 8 Calculs
    10
  • 9 Expression des résultats
    11
  • 10 Fidélité
    11
  • 11 Rapport
    11
  • Annexe A (informative) Temps de rétention relatifs par rapport à l'éthylbenzène-D10 des hydrocarbures aromatiques volatils et des hydrocarbures halogénés volatils sur les colonnes suivantes: CP-Sil 5 CB et CP-Sil 13 CB
    12
  • Annexe B (informative) Validation
    13
  • Bibliographie
    17
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