NF ISO 23275-1
Animal and vegetable fats and oils - Cocoa butter equivalents in cocoa butter and plain chocolate - Part 1 : détermination of the presence of cocoa butter equivalents
ISO 23275-1:2006 specifies a procedure for the detection of cocoa butter equivalents (CBEs) in cocoa butter and plain chocolate by high-resolution capillary gas liquid chromatography of triacylglycerols and subsequent data evaluation by regression analysis. The method is applicable for the detection of 2 % CBE admixture to cocoa butter, corresponding to about 0,6 % CBE in chocolate (i.e. the assumed fat content of chocolate is 30 %).
ISO 23275-1:2006 specifies a procedure for the detection of cocoa butter equivalents (CBEs) in cocoa butter and plain chocolate by high-resolution capillary gas liquid chromatography of triacylglycerols and subsequent data evaluation by regression analysis.
The method is applicable for the detection of 2 % CBE admixture to cocoa butter, corresponding to about 0,6 % CBE in chocolate (i.e. the assumed fat content of chocolate is 30 %).
<p>ISO 23275-1:2006 specifies a procedure for the detection of cocoa butter equivalents (CBEs) in cocoa butter and plain chocolate by high-resolution capillary gas liquid chromatography of triacylglycerols and subsequent data evaluation by regression analysis. </p> <p>The method is applicable for the detection of 2 % CBE admixture to cocoa butter, corresponding to about 0,6 % CBE in chocolate (i.e. the assumed fat content of chocolate is 30 %).</p>
- Avant-proposiv
- Introductionv
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1 Domaine d'application1
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2 Termes et définitions1
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3 Principe1
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4 Réactifs et matériaux1
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5 Appareillage2
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6 Échantillonnage3
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7 Préparation de l'échantillon pour essai3
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7.1 Préparation du MRC beurre de cacao pour étalonnage et vérification de l'aptitude du système3
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7.2 Préparation de l'échantillon de chocolat3
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8 Mode opératoire3
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8.1 Extraction de la matière grasse3
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8.2 Séparation des triacylglycérols individuels par HR-GC3
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8.3 Identification4
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9 Calculs4
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9.1 Détermination des facteurs de réponse4
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9.2 Calcul des pourcentages des triacylglycérols4
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9.3 Décision relative à la pureté en beurre de cacao de l'échantillon5
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10 Exigences du mode opératoire5
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10.1 Considérations générales5
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10.2 Aptitude du système5
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11 Fidélité6
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11.1 Essai interlaboratoires6
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11.2 Répétabilité6
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11.3 Reproductibilité6
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12 Rapport d'essai6
- Annexe A (informative) Résultats d'un essai interlaboratoires7
- Bibliographie13
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