NF ISO 23655-1

NF ISO 23655-1

October 2022
Standard Current

Water quality - Nickel-59 and nickel-63 - Part 1 : test method using liquid scintillation counting

This document specifies the determination of nickel-59 and nickel-63 (59Ni and 63Ni) activity concentration in samples of all types of water using liquid scintillation counting (LSC). Using currently available liquid scintillation counters, this test method can measure 59Ni activity concentrations of 50 mBq·l−1 and 63Ni activity concentrations of 20 mBq·l−1 with a counting time of 200 min and a sample volume of 1,5 l.NOTE      These performance indicators are wholly dependent on the measurement regimes in individual laboratories; in particular, the detection limits for 59Ni are entirely dependent on the levels of 63Ni that can be present.The range of application depends on the amount of dissolved material in the water and on the performance characteristics of the measurement equipment (background count rate and detection efficiency).It is the laboratory’s responsibility to ensure the suitability of this test method for the water samples tested.

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Main informations

Collections

National standards and national normative documents

Publication date

October 2022

Number of pages

32 p.

Reference

NF ISO 23655-1

ICS Codes

13.060.60   Examination of physical properties of water
17.240   Radiation measurements

Classification index

M60-838-1

Print number

1

International kinship

Sumary
Water quality - Nickel-59 and nickel-63 - Part 1 : test method using liquid scintillation counting

This document specifies the determination of nickel-59 and nickel-63 (59Ni and 63Ni) activity concentration in samples of all types of water using liquid scintillation counting (LSC). Using currently available liquid scintillation counters, this test method can measure 59Ni activity concentrations of 50 mBq·l−1 and 63Ni activity concentrations of 20 mBq·l−1 with a counting time of 200 min and a sample volume of 1,5 l.

NOTE      These performance indicators are wholly dependent on the measurement regimes in individual laboratories; in particular, the detection limits for 59Ni are entirely dependent on the levels of 63Ni that can be present.

The range of application depends on the amount of dissolved material in the water and on the performance characteristics of the measurement equipment (background count rate and detection efficiency).

It is the laboratory’s responsibility to ensure the suitability of this test method for the water samples tested.

Table of contents
  • 1 Domaine d'application
  • 2 Références normatives
  • 3 Termes et définitions
  • 4 Symboles généraux et symboles spécifiques du nickel 59 et du nickel
    63
  • 5 Principe
  • 6 Réactifs
  • 7 Équipement
  • 8 Échantillonnage
  • 9 Mise en place et étalonnage des scintillations en milieu liquide
  • 10 Mode opératoire
  • 11 Contrôle de la qualité
  • 12 Expression des résultats
  • 13 Rapport d'essai
  • Annexe A Séparation et purification du nickel
  • Bibliographie
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