NF ISO 3987

NF ISO 3987

December 2016
Standard Cancelled

Petroleum products - Determination of sulfated ash in lubricating oils and additives

ISO 3987:2010 describes a procedure for the determination of the mass percentage of sulfated ash from unused lubricating oils containing additives and from additive concentrates used in compounding. These additives usually contain one or more of the following metals: barium, calcium, magnesium, zinc, potassium, sodium and tin. The elements sulfur, phosphorus and chlorine can also be present in combined form.

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Main informations

Collections

National standards and national normative documents

Publication date

December 2016

Number of pages

13 p.

Reference

NF ISO 3987

ICS Codes

75.100   Lubricants, industrial oils and related products

Classification index

T60-143

Print number

1

International kinship

Sumary
Petroleum products - Determination of sulfated ash in lubricating oils and additives

ISO 3987:2010 describes a procedure for the determination of the mass percentage of sulfated ash from unused lubricating oils containing additives and from additive concentrates used in compounding. These additives usually contain one or more of the following metals: barium, calcium, magnesium, zinc, potassium, sodium and tin. The elements sulfur, phosphorus and chlorine can also be present in combined form.

Replaced standards (1)
NF ISO 3987
May 1999
Standard Cancelled
Petroleum products. Lubricating oils and additives. Determination of sulfated ash.

Standard replaced by (1)
NF ISO 3987
October 2024
Standard Current
Petroleum products - Determination of sulfated ash in lubricating oils and additives and fatty acid methyl esters

This document describes a procedure for the determination of the mass percentage of sulfated ash from unused lubricating oils containing additives and from additive concentrates used in compounding. These additives usually contain one or more of the following metals: barium, calcium, magnesium, zinc, potassium, sodium and tin. The elements sulfur, phosphorus and chlorine can also be present in combined form. This document is also applicable to fatty acid methyl esters (FAME). This test method is applicable to products having sulphated ash contents in the range mass fraction of 0,005 % to 25,00 %. Application of this procedure to sulfated ash levels below a mass fraction of 0,02 % is restricted to oil products containing ashless additives. This document is not intended for the analysis of used engine oils containing lead, nor for the analysis of non-additive lubricating oils, for which ISO 6245 is suitable.

Table of contents
  • Avant-propos
  • 1 Domaine d'application
  • 2 Références normatives
  • 3 Termes et définitions
  • 4 Principe
  • 5 Réactifs
  • 6 Appareillage
  • 7 Échantillons et échantillonnage
  • 8 Mode opératoire
  • 9 Calculs
  • 10 Expression des résultats
  • 11 Fidélité
  • 12 Rapport d'essai
  • Bibliographie
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