FD ISO/TR 22971
Accuracy (trueness and precision) of measurement methods and results - Practical guidance for use of ISO 5725-2:1994 in designing, implementing and statistically analysing interlaboratory repeatability and reproducibility results
ISO/TR 22971:2005 provides users with practical guidance to the use of ISO 5725-2:1994 and presents simplified step-by-step procedures for the design, implementation, and statistical analysis of inter-laboratory studies for assessing the variability of a standard measurement method and on the determination of repeatability and reproducibility of data obtained in inter-laboratory testing.
ISO/TR 22971:2005 provides users with practical guidance to the use of ISO 5725-2:1994 and presents simplified step-by-step procedures for the design, implementation, and statistical analysis of inter-laboratory studies for assessing the variability of a standard measurement method and on the determination of repeatability and reproducibility of data obtained in inter-laboratory testing.
- Avant-proposiv
- Introductionv
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1 Domaine d'application1
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2 Organisation d'un programme interlaboratoires1
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2.1 Exigences relatives à une expérience de fidélité1
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2.2 Responsabilités du personnel impliqué dans une expérience de fidélité2
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3 Examen critique des données3
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3.1 Description des données3
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3.2 Tests des valeurs aberrantes7
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3.3 Conclusions9
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4 Estimation des écarts-types de répétabilité et de reproductibilité11
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4.1 Analyse de variance11
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4.2 Description du modèle11
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4.3 Exemples13
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4.4 Utilisation des limites de répétabilité et de reproductibilité15
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5 Exemples traités avec des progiciels statistiques16
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5.1 Généralités16
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5.2 Détermination de la teneur en soufre du charbon16
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5.3 Titrage thermométrique de créosote24
- Annexe A (normative) Symboles et abréviations30
- Bibliographie33
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