FD T16-203

FD T16-203

December 2011
Published document Current

Nanotechnologies - Characterization of single-wall carbon nanotubes using scanning electron microscopy and energy dispersive X-ray spectrometry analysis

ISO/TS 10798:2011 establishes methods to characterize the morphology, and to identify the elemental composition of catalysts and other inorganic impurities in raw and purified single-wall carbon nanotube (SWCNT) powders and films, using scanning electron microscopy and energy dispersive X-ray spectrometry analysis. The methods described in ISO/TS 10798:2011 for SWCNTs can also be applied to the analysis of multiwall carbon nanotubes (MWCNTs).

See more
View the extract
Main informations

Collections

National standards and national normative documents

Publication date

December 2011

Number of pages

34 p.

Reference

FD T16-203

ICS Codes

07.120   Nanotechnologies

Classification index

T16-203

Print number

1 - 10/01/2012

International kinship

ISO/TS 10798:2011
Sumary
Nanotechnologies - Characterization of single-wall carbon nanotubes using scanning electron microscopy and energy dispersive X-ray spectrometry analysis

ISO/TS 10798:2011 establishes methods to characterize the morphology, and to identify the elemental composition of catalysts and other inorganic impurities in raw and purified single-wall carbon nanotube (SWCNT) powders and films, using scanning electron microscopy and energy dispersive X-ray spectrometry analysis.

The methods described in ISO/TS 10798:2011 for SWCNTs can also be applied to the analysis of multiwall carbon nanotubes (MWCNTs).

Table of contents
View the extract
  • Avant-propos
    iv
  • Introduction
    v
  • 1 Domaine d'application
    1
  • 2 Références normatives
    1
  • 3 Termes et définitions
    1
  • 3.1 Microscopie électronique à balayage
    1
  • 3.2 Termes relatifs à l'analyse par microsonde électronique
    2
  • 3.3 Termes relatifs à l'échantillonnage
    4
  • 4 Principes généraux
    4
  • 4.1 Analyse MEB
    4
  • 4.2 Analyse EDX
    5
  • 4.3 Applicabilité à l'analyse de MWCNT
    5
  • 4.4 Autres méthodes d'analyse auxiliaires
    5
  • 5 Méthodes de préparation de l'échantillon
    5
  • 5.1 Consignes et mesures de sécurité
    5
  • 5.2 Préparation des échantillons pour les analyses par MEB/EDX
    6
  • 5.3 Préparation de l'échantillon MEB/techniques de fixation
    6
  • 6 Modes opératoires de mesure
    8
  • 6.1 Analyse MEB
    8
  • 6.2 Analyse EDX
    9
  • 7 Analyse des données et interprétation des résultats
    10
  • 7.1 Résultats obtenus par MEB
    10
  • 7.2 Résultats obtenus par EDX
    10
  • 8 Incertitude de mesure
    10
  • 8.1 Analyse MEB
    10
  • 8.2 Analyse EDX
    10
  • Annexe A (normative) Méthodes d'échantillonnage pour MEB
    12
  • Annexe B (informative) Informations auxiliaires sur la caractérisation par EDX des matériaux de NTC
    14
  • Annexe C (informative) Étude de cas pour l'analyse d'échantillons de SWCNT synthétisés et purifiés
    16
  • Annexe D (informative) Exemples d'analyse MEB/EDX de SWCNT
    23
  • Bibliographie
    27
ZOOM ON ... the Requirements department
To comply with a standard, you need to quickly understand its issues in order to determine its impact on your activity.

The Requirements department helps you quickly locate within the normative text:
- mandatory clauses to satisfy,
- non-essential but useful clauses to know, such as permissions and recommendations.

The identification of these types of clauses is based on the document “ISO / IEC Directives, Part 2 - Principles and rules of structure and drafting of ISO documents ”as well as on a constantly enriched list of verbal forms.

With Requirements, quickly access the main part of the normative text!

With Requirements, quickly access the main part of the normative text!
Need to identify, monitor and decipher standards?

COBAZ is the simple and effective solution to meet the normative needs related to your activity, in France and abroad.

Available by subscription, CObaz is THE modular solution to compose according to your needs today and tomorrow. Quickly discover CObaz!

Request your free, no-obligation live demo

I discover COBAZ