NF EN ISO 15009

NF EN ISO 15009

May 2016
Standard Current

Soil quality - Gas chromatographic determination of the content of volatile aromatic hydrocarbons, naphthalene and volatile halogenated hydrocarbons - Purge-and-trap method with thermal desorption

ISO 15009:2016 specifies a method for quantitative gas-chromatographic determination of volatile aromatic hydrocarbons, naphthalene and volatile halogenated hydrocarbons in soil.This International Standard is applicable to all types of soil.NOTE In the case of unsaturated peaty soils, absorption of the extraction solution may occur.The lower limit of quantification is dependent on the equipment used and the quality of the methanol grade used for the extraction of the soil sample.Under the conditions specified in this International Standard the following limits of quantification apply (expressed on basis of dry matter):Typical limit of quantification when using GC-FID:- Volatile aromatic hydrocarbons: 0,1 mg/kgTypical limit of quantification when using GC-ECD:- Volatile halogenated hydrocarbons: 0,01 mg/kgLower limits of quantification for some compounds can be achieved by using mass spectrometry (MS) with selected ion detection.

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Main informations

Collections

National standards and national normative documents

Publication date

May 2016

Number of pages

26 p.

Reference

NF EN ISO 15009

ICS Codes

13.080.10   Chemical characteristics of soils

Classification index

X31-426

Print number

1

International kinship

ISO 15009:2016

European kinship

EN ISO 15009:2016
Sumary
Soil quality - Gas chromatographic determination of the content of volatile aromatic hydrocarbons, naphthalene and volatile halogenated hydrocarbons - Purge-and-trap method with thermal desorption

ISO 15009:2016 specifies a method for quantitative gas-chromatographic determination of volatile aromatic hydrocarbons, naphthalene and volatile halogenated hydrocarbons in soil.

This International Standard is applicable to all types of soil.

NOTE In the case of unsaturated peaty soils, absorption of the extraction solution may occur.

The lower limit of quantification is dependent on the equipment used and the quality of the methanol grade used for the extraction of the soil sample.

Under the conditions specified in this International Standard the following limits of quantification apply (expressed on basis of dry matter):

Typical limit of quantification when using GC-FID:

- Volatile aromatic hydrocarbons: 0,1 mg/kg

Typical limit of quantification when using GC-ECD:

- Volatile halogenated hydrocarbons: 0,01 mg/kg

Lower limits of quantification for some compounds can be achieved by using mass spectrometry (MS) with selected ion detection.

Replaced standards (1)
NF EN ISO 15009
July 2013
Standard Cancelled
Soil quality - Gas chromatographic determination of the content of volatile aromatic hydrocarbons, naphthalene and volatile halogenated hydrocarbons - Purge-and-trap method with thermal desorption

Le présent document spécifie une méthode pour la détermination quantitative par chromatographie en phase gazeuse des hydrocarbures volatils, du naphtalène et des hydrocarbures halogénés volatils contenus dans les sols.

Table of contents
  • 1 Domaine d'application
  • 2 Références normatives
  • 3 Principe
  • 4 Réactifs
  • 5 Appareillage
  • 6 Échantillonnage, conservation et traitement préliminaire des échantillons
  • 7 Mode opératoire
  • 8 Calcul
  • 9 Expression des résultats
  • 10 Fidélité
  • 11 Rapport d'essai
  • Annexe A Temps de rétention relatifs par rapport à l'éthylbenzène-D10 des hydrocarbures aromatiques volatils et des hydrocarbures halogénés volatils sur les colonnes suivantes: CP-Sil 5 CB et CP-Sil 13 CB
  • Annexe B Vérification des étalons internes
  • Annexe C Validation
  • Annexe D Informations sur les instruments de purge et de piégeage
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