NF EN ISO 15753

NF EN ISO 15753

June 2016
Standard Current

Animal and vegetable fats and oils - Determination of polycyclic aromatic hydrocarbons

ISO 15753:2016 describes two methods for the determination of 15 polycyclic aromatic hydrocarbons (PAHs) in animal and vegetable fats and oils: - a general method; - a specific method for coconut oil and vegetable oils with short-chain fatty acids. These methods are not quantitative for the very volatile compounds such as naphthalene, acenaphthene and fluorene. Due to interferences provided by the matrix itself, palm oil and olive pomace oil cannot be analysed using this method. The quantification limit is 0,2 µg/kg for almost all compounds analysed, except for fluoranthene and benzo(g,h,i)perylene, where the quantification limit is 0,3 µg/kg, and indeno(1,2,3-c,d)pyrene, where the quantification limit is 1,0 µg/kg. NOTE The results for olive pomace oil in Annex B show that this method is not applicable to this type of oil. The precision data determined are very poor. Milk and milk products (or fat coming from milk and milk products) are excluded from the scope of this International Standard.

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Main informations

Collections

National standards and national normative documents

Publication date

June 2016

Number of pages

29 p.

Reference

NF EN ISO 15753

ICS Codes

67.200.10   Animal and vegetable fats and oils

Classification index

T60-267

Print number

1

International kinship

European kinship

EN ISO 15753:2016
Sumary
Animal and vegetable fats and oils - Determination of polycyclic aromatic hydrocarbons

ISO 15753:2016 describes two methods for the determination of 15 polycyclic aromatic hydrocarbons (PAHs) in animal and vegetable fats and oils:

- a general method;

- a specific method for coconut oil and vegetable oils with short-chain fatty acids.

These methods are not quantitative for the very volatile compounds such as naphthalene, acenaphthene and fluorene. Due to interferences provided by the matrix itself, palm oil and olive pomace oil cannot be analysed using this method.

The quantification limit is 0,2 µg/kg for almost all compounds analysed, except for fluoranthene and benzo(g,h,i)perylene, where the quantification limit is 0,3 µg/kg, and indeno(1,2,3-c,d)pyrene, where the quantification limit is 1,0 µg/kg.

NOTE The results for olive pomace oil in Annex B show that this method is not applicable to this type of oil. The precision data determined are very poor.

Milk and milk products (or fat coming from milk and milk products) are excluded from the scope of this International Standard.

Replaced standards (2)
NF EN ISO 15753
November 2006
Standard Cancelled
Animal and vegetable fats and oils - Determination of polycyclic aromatic hydrocarbons

<p>ISO 15753:2006 describes two methods for the determination of 15 polycyclic aromatic hydrocarbons (PAHs) in animal and vegetable fats and oils: a general method, and a method specific for coconut oil and short-chain vegetable oils.</p> <p>These methods are not quantitative for the very volatile compounds such as naphthalene, acenaphthene and fluorene. Due to interferences provided by the matrix itself, palm oil and olive pomace oil cannot be analysed using this method.</p>

NF EN ISO 15753/A1
September 2011
Standard Cancelled
Animal and vegetable fats and oils - Determination of polycyclic aromatic hydrocarbons - Amendment 1 : exclusion of olive pomace oil from the scope

Le présent document décrit deux méthodes pour la détermination de 15 hydrocarbures aromatiques polycycliques (HAP) dans les corps gras d'origines animale et végétale. Cet amendement exclu l'huile de grignons d'olive de son domaine d'application.

Table of contents
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  • 1 Domaine d'application
  • 2 Références normatives
  • 3 Termes et définitions
  • 4 Principe
  • 5 Réactifs et matériaux
  • 6 Appareillage
  • 7 Échantillonnage
  • 8 Préparation de l'échantillon
  • 9 Mode opératoire pour la détermination des HAP à partir des corps gras: Méthode générale
  • 10 Mode opératoire pour la détermination des HAP à partir des corps gras: Méthode spécifique pour l'huile de coprah
  • 11 Chromatographie liquide à haute performance (CLHP)
  • 12 Expression des résultats
  • 13 Fidélité
  • 14 Rapport d'essai
  • Annexe A Valeurs des taux de récupération, schémas fonctionnels, chromatogrammes et séquences d'injection
  • Annexe B Résultats de l'essai interlaboratoires
  • Bibliographie
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