NF EN ISO 22036

NF EN ISO 22036

January 2024
Standard Current

Environmental solid matrices - Determination of elements using inductively coupled plasma optical emission spectrometry (ICP-OES)

This document specifies a method for the determination of the following elements in aqua regia, nitric acid or mixture of hydrochloric (HCl), nitric (HNO3) and tetrafluoroboric (HBF4)/hydrofluoric (HF) acid digests of soil, treated biowaste, waste, sludge and sediment:Aluminium (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), bismuth (Bi), boron (B), cadmium (Cd), calcium (Ca), cerium (Ce), chromium (Cr), cobalt (Co), copper (Cu), dysprosium (Dy), erbium (Er), europium (Eu), gallium (Ga), gadolinium (Gd), germanium (Ge), gold (Au), hafnium (Hf), holmium (Ho), indium (In), iridium (Ir), iron (Fe), lanthanum (La), lead (Pb), lithium (Li), lutetium (Lu) magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), neodymium (Nd), nickel (Ni), palladium (Pd), phosphorus (P), platinum (Pt), potassium (K), praseodymium (Pr), rhodium (Rh), ruthenium (Ru), samarium (Sm), scandium (Sc), selenium (Se), silicon (Si), silver (Ag), sodium (Na), strontium (Sr), sulfur (S), tantalum (Ta), tellurium (Te), terbium (Tb), thallium (Tl), thulium (Tm), thorium (Th), tin (Sn), titanium (Ti), tungsten (W), vanadium (V), yttrium (Y), ytterbium (Yb), zinc (Zn) and zirconium (Zr).The method is also applicable to other extracts or digests originating from, for example, DTPA extraction, fusion methods or total digestion methods, provided the user has verified the applicability.The method has been validated for the elements given in Table A.1 (sludge), Table A.2 (compost) and Table A.3 (soil). The method is applicable for other solid matrices and other elements as listed above, provided the user has verified the applicability.This method is also applicable for the determination of major, minor and trace elements in aqua regia and nitric acid digests and in eluates of construction products (EN 17200[22]).NOTE            Construction products include e.g. mineral-based products; bituminous products; metals; wood-based products; plastics and rubbers; sealants and adhesives; paints and coatings.

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Publication date

January 2024

Number of pages

38 p.

Reference

NF EN ISO 22036

ICS Codes

13.030.01   Wastes in general
13.080.10   Chemical characteristics of soils

Classification index

X31-420

Print number

1

International kinship

ISO 22036:2024

European kinship

EN ISO 22036:2024
Sumary
Environmental solid matrices - Determination of elements using inductively coupled plasma optical emission spectrometry (ICP-OES)

This document specifies a method for the determination of the following elements in aqua regia, nitric acid or mixture of hydrochloric (HCl), nitric (HNO3) and tetrafluoroboric (HBF4)/hydrofluoric (HF) acid digests of soil, treated biowaste, waste, sludge and sediment:

Aluminium (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), bismuth (Bi), boron (B), cadmium (Cd), calcium (Ca), cerium (Ce), chromium (Cr), cobalt (Co), copper (Cu), dysprosium (Dy), erbium (Er), europium (Eu), gallium (Ga), gadolinium (Gd), germanium (Ge), gold (Au), hafnium (Hf), holmium (Ho), indium (In), iridium (Ir), iron (Fe), lanthanum (La), lead (Pb), lithium (Li), lutetium (Lu) magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), neodymium (Nd), nickel (Ni), palladium (Pd), phosphorus (P), platinum (Pt), potassium (K), praseodymium (Pr), rhodium (Rh), ruthenium (Ru), samarium (Sm), scandium (Sc), selenium (Se), silicon (Si), silver (Ag), sodium (Na), strontium (Sr), sulfur (S), tantalum (Ta), tellurium (Te), terbium (Tb), thallium (Tl), thulium (Tm), thorium (Th), tin (Sn), titanium (Ti), tungsten (W), vanadium (V), yttrium (Y), ytterbium (Yb), zinc (Zn) and zirconium (Zr).

The method is also applicable to other extracts or digests originating from, for example, DTPA extraction, fusion methods or total digestion methods, provided the user has verified the applicability.

The method has been validated for the elements given in Table A.1 (sludge), Table A.2 (compost) and Table A.3 (soil). The method is applicable for other solid matrices and other elements as listed above, provided the user has verified the applicability.

This method is also applicable for the determination of major, minor and trace elements in aqua regia and nitric acid digests and in eluates of construction products (EN 17200[22]).

NOTE            Construction products include e.g. mineral-based products; bituminous products; metals; wood-based products; plastics and rubbers; sealants and adhesives; paints and coatings.

Replaced standards (2)
NF EN 16170
December 2016
Standard Cancelled
Sludge, treated biowaste and soil - Determination of elements using inductively coupled plasma optical emission spectrometry (ICP-OES)

Le présent document spécifie une méthode de détermination des éléments suivants dans des digestats d'eau régale ou d'acide nitrique de boues, de bio-déchets traités et de sols : Aluminium (Al) , antimoine (Sb) , arsenic (As) , baryum (Ba) , béryllium (Be) , bismuth (Bi) , bore (B) , cadmium (Cd) , calcium (Ca) , cérium (Ce) , chrome (Cr) , cobalt (Co) , cuivre (Cu) , gallium (Ga) , indium (In) , fer (Fe) , lanthane (La) , plomb (Pb) , lithium (Li) , magnésium (Mg) , manganèse (Mn) , mercure (Hg) , molybdène (Mo) , néodyme (Nd) , nickel (Ni) , phosphore (P) , potassium (K) , praséodyme (Pr) , samarium (Sm) , scandium (Sc) , sélénium (Se) , silicium (Si) , argent (Ag) , sodium (Na) , strontium (Sr) , soufre (S) , tellure (Te) , thallium (Tl) , thorium (Th) , étain (Sn) , titane (Ti) , tungstène (W) , uranium (U) , vanadium (V) , zinc (Zn) et zirconium (Zr) . La présente méthode a été validée pour les éléments donnés dans le Tableau A.1. Cette méthode est applicable pour les autres éléments énumérés ci-dessus, sous réserve que l'utilisateur en ait vérifié l'applicabilité.

NF ISO 22036
February 2009
Standard Current
Soil quality - Determination of trace elements in extracts of soil by inductively coupled plasma-atomic emission spectrometry (ICP-AES)

ISO 22036:2008 describes the determination of trace elements in digests or extraction solutions from soil by inductively coupled plasma - atomic emission spectrometry (ICP-AES) for 34 elements. This multi-element determination method is applicable to soil extracts obtained with aqua regia in accordance with ISO 11466, with DTPA in accordance with ISO 14870 or other weak extractants, or soil extracts for the determination of total element contents using the acid digestion method of ISO 14869-1 or the fusion method of ISO 14869-2. The choice of calibration method depends on the extractant and can be adapted to the extractant concentration.

Table of contents
  • 1 Domaine d'application
  • 2 Références normatives
  • 3 Termes et définitions
  • 4 Principe
  • 5 Interférences
  • 6 Réactifs
  • 7 Appareillage
  • 8 Mode opératoire
  • 9 Calcul
  • 10 Expression des résultats
  • 11 Caractéristiques de performance
  • 12 Rapport d'essai
  • A Données de répétabilité et de reproductibilité
  • B Longueurs d'onde et limites de détection instrumentales estimées
  • C Correction inter-éléments
  • Bibliographie
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