NF EN ISO 22155
NF EN ISO 22155

NF EN ISO 22155

May 2016
Standard Current

Soil quality - Gas chromatographic determination of volatile aromatic and halogenated hydrocarbons and selected ethers - Static headspace method

ISO 22155:2016 specifies a static headspace method for quantitative gas chromatographic determination of volatile aromatic and halogenated hydrocarbons and selected aliphatic ethers in soil.ISO 22155:2016 is applicable to all types of soil.The limit of quantification is dependent on the detection system used and the quality of the methanol grade used for the extraction of the soil sample.Under the conditions specified in this International Standard, the following limits of quantifications apply (expressed on basis of dry matter).Typical limit of quantification when using GC-FID:- volatile aromatic hydrocarbons: 0,2 mg/kg;- aliphatic ethers as methyl tert.-butyl ether(MTBE) and tert.-amyl methyl ether (TAME): 0,5 mg/kg.Typical limit of quantification when using GC-ECD:- volatile halogenated hydrocarbons: 0,01 mg/kg to 0,2 mg/kg.Lower limits of quantification for some compounds can be achieved by using mass spectrometry (MS) with selected ion detection (see Annex D).

Main informations

Collections

National standards and national normative documents

Publication date

May 2016

Number of pages

29 p.

Reference

NF EN ISO 22155

ICS Codes

13.080.10   Chemical characteristics of soils

Classification index

X31-438

Print number

1

International kinship

ISO 22155:2016

European kinship

EN ISO 22155:2016
Sumary
Soil quality - Gas chromatographic determination of volatile aromatic and halogenated hydrocarbons and selected ethers - Static headspace method

ISO 22155:2016 specifies a static headspace method for quantitative gas chromatographic determination of volatile aromatic and halogenated hydrocarbons and selected aliphatic ethers in soil.

ISO 22155:2016 is applicable to all types of soil.

The limit of quantification is dependent on the detection system used and the quality of the methanol grade used for the extraction of the soil sample.

Under the conditions specified in this International Standard, the following limits of quantifications apply (expressed on basis of dry matter).

Typical limit of quantification when using GC-FID:

- volatile aromatic hydrocarbons: 0,2 mg/kg;

- aliphatic ethers as methyl tert.-butyl ether(MTBE) and tert.-amyl methyl ether (TAME): 0,5 mg/kg.

Typical limit of quantification when using GC-ECD:

- volatile halogenated hydrocarbons: 0,01 mg/kg to 0,2 mg/kg.

Lower limits of quantification for some compounds can be achieved by using mass spectrometry (MS) with selected ion detection (see Annex D).

Replaced standards (1)
NF EN ISO 22155
NF EN ISO 22155
April 2013
Standard Cancelled
Soil quality - Gas chromatographic determination of volatile aromatic and halogenated hydrocarbons and selected ethers - Static headspace method

Table of contents
  • 1 Domaine d'application
  • 2 Références normatives
  • 3 Principe
  • 4 Réactifs
  • 5 Appareillage
  • 6 Échantillonnage, conservation et traitement préliminaire des échantillons
  • 7 Mode opératoire
  • 8 Calculs
  • 9 Expression des résultats
  • 10 Fidélité
  • 11 Rapport d'essai
  • Annexe A Temps de rétention relatifs par rapport à l'éthylbenzène-D10 des hydrocarbures aromatiques volatils et des hydrocarbures halogénés volatils - Exemples d'ions cibles et qualifiants adaptés
  • Annexe B Vérification sur des étalons internes
  • Annexe C Validation (généralités)
  • Annexe D Caractéristiques de performance
  • Bibliographie
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