NF EN ISO 5764
Milk - Determination of freezing point - Thermistor cryoscope method (Reference method)
ISO 5764|IDF 108:2009 specifies a reference method for the determination of the freezing point of raw bovine milk, heat-treated whole, reduced fat and skimmed bovine milk, as well as raw ovine and caprine milk, by using a thermistor cryoscope.The freezing point can be used to estimate the proportion of extraneous water in milk. Calculation of the amount of extraneous water is subject to daily and seasonal variations, and is not within the scope of ISO 5764|IDF 108:2009.Results obtained from samples with a titratable acidity exceeding 20 ml of 0,1 mol/l sodium hydroxide solution per 10 g of non-fat solids are not representative of the original milk.
ISO 5764|IDF 108:2009 specifies a reference method for the determination of the freezing point of raw bovine milk, heat-treated whole, reduced fat and skimmed bovine milk, as well as raw ovine and caprine milk, by using a thermistor cryoscope.
The freezing point can be used to estimate the proportion of extraneous water in milk. Calculation of the amount of extraneous water is subject to daily and seasonal variations, and is not within the scope of ISO 5764|IDF 108:2009.
Results obtained from samples with a titratable acidity exceeding 20 ml of 0,1 mol/l sodium hydroxide solution per 10 g of non-fat solids are not representative of the original milk.
ISO 5764|IDF 108:2002 specifies a reference method for the determination of the freezing point of raw, pasteurized, UHT-treated or sterilized whole milk, partially skimmed milk and skimmed milk by using a thermistor cryoscope. The freezing point can be used for estimating the proportion of extraneous water in milk. Calculation of the amount of extraneous water is complicated by daily variation, seasonal variation, etc. and is not within the scope of ISO 5764¦IDF 108:2002. Results obtained from samples with a titratable acidity exceeding 20 ml of 0,1 mol/l sodium hydroxide solution per 10 g of non-fat solids will not be representative of the original milk.
- Avant-proposiv
- Avant-proposv
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1 Domaine d'application1
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2 Références normatives1
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3 Termes et définitions1
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4 Principe2
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5 Réactifs2
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6 Appareillage3
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7 Échantillonnage4
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8 Étalonnage du cryoscope à thermistance5
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9 Préparation de l'échantillon pour essai6
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9.1 Préparation6
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9.2 État de l'échantillon6
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10 Mode opératoire6
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10.1 Vérifications préliminaires6
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10.2 Vérification de routine de l'étalonnage6
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10.3 Détermination6
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11 Calcul et expression des résultats7
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11.1 Calculs7
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11.2 Expression des résultats7
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12 Fidélité7
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12.1 Essai interlaboratoires7
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12.2 Répétabilité8
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12.3 Reproductibilité8
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13 Rapport d'essai8
- Annexe A (informative) Essai interlaboratoires du lait de bovin9
- Annexe B (informative) Essai interlaboratoires du lait cru de brebis et de chèvre11
- Annexe C (informative) Lignes directrices pour l'application de méthodes de routine au cryoscope à thermistance13
- Annexe D (informative) Ajustement du point de congélation utilisé comme référence pour le lait véritable16
- Bibliographie17
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