NF ISO 11929

NF ISO 11929

May 2010
Standard Cancelled mandatory application standard

Determination of the characteristic limits (decision threshold, detection limit and limits of the confidence interval) for measurements of ionizing radiation - Fundamentals and application

ISO 11929:2010 specifies a procedure, in the field of ionizing radiation metrology, for the calculation of the "decision threshold", the "detection limit" and the "limits of the confidence interval" for a non-negative ionizing radiation measurand, when counting measurements with preselection of time or counts are carried out, and the measurand results from a gross count rate and a background count rate as well as from further quantities on the basis of a model of the evaluation. In particular, the measurand can be the net count rate as the difference of the gross count rate and the background count rate, or the net activity of a sample. It can also be influenced by calibration of the measuring system, by sample treatment and by other factors.

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Main informations

Collections

National standards and national normative documents

Publication date

May 2010

Number of pages

67 p.

Reference

NF ISO 11929

ICS Codes

17.240   Radiation measurements

Classification index

M60-200

Print number

1 - 26/05/2010

International kinship

Sumary
Determination of the characteristic limits (decision threshold, detection limit and limits of the confidence interval) for measurements of ionizing radiation - Fundamentals and application

ISO 11929:2010 specifies a procedure, in the field of ionizing radiation metrology, for the calculation of the "decision threshold", the "detection limit" and the "limits of the confidence interval" for a non-negative ionizing radiation measurand, when counting measurements with preselection of time or counts are carried out, and the measurand results from a gross count rate and a background count rate as well as from further quantities on the basis of a model of the evaluation. In particular, the measurand can be the net count rate as the difference of the gross count rate and the background count rate, or the net activity of a sample. It can also be influenced by calibration of the measuring system, by sample treatment and by other factors.

Replaced standards (4)
NF ISO 11929-5
December 2005
Standard Cancelled
Determination of the detection limit and decision threshold for ionizing radiation measurements - Part 5 : fundamentals and applications to counting measurements on filters during accumulation of radioactive materiel

ISO 11929-5:2004 specifies suitable statistical values which allow an assessment of the detection capabilities in ionizing radiation measurements and of the physical effect quantified by the measurand. For this purpose, Bayesian statistical methods are used to specify characteristic limits. ISO 11929-5:2004 deals with fundamentals and applications to counting measurements on filters during accumulation of radioactive material.

NF ISO 11929-6
December 2005
Standard Cancelled
Determination of the detection limit and decision threshold for ionizing radiation measurements - Part 6 : fundamentals and applications to measurements by use of transient mode

ISO 11929-6:2005 specifies suitable statistical values which allow an assessment of the detection capabilities in ionizing radiation measurements by use of a transient mode. For this purpose, statistical methods are used to specify two statistical values characterizing given probabilities of error. ISO 11929-6:2005 deals with fundamentals and applications to measurements by use of transient mode.

NF ISO 11929-7
November 2005
Standard Cancelled
Determination of the detection limit and decision threshold for ionizing radiation measurements - Part 7 : fundamentals and general applications

Le présent document présente les principes statistiques pour la détermination de la limite de détection, du seuil de décision et des limites de l'intervalle de confiance pour des applications générales de mesurages des rayonnements ionisants.

NF ISO 11929-8
November 2005
Standard Cancelled
Determination of the detection limit and decision threshold for ionizing radiation measurements - Part 8 : fundamentals and application to unfolding of spectrometric measurements without the influence of sample treatment

ISO 11929-8:2005 specifies a method for determination of suitable statistical values which allow an assessment of the detection capabilities in spectrometric nuclear radiation measurements, and of the physical effect quantified by a measurand (for example, a net area of a spectrometric line in an alpha- or gamma-spectrum) which is determined by evaluation of a multi-channel spectrum by unfolding methods, without the influence of sample treatment. For this purpose, Bayesian statistical methods are used to specify characteristic limits.

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Standard replaced by (4)
NF ISO 11929-1
September 2020
Standard Cancelled
Determination of the characteristic limits (decision threshold, detection limit and limits of the coverage interval) for measurements of ionizing radiation - Fundamentals and application - Part 1 : elementary applications

Le présent document couvre les applications de base des mesurages par comptage souvent utilisés dans le domaine de la métrologie des rayonnements ionisants. Il se limite aux applications pour lesquelles il est possible d'évaluer les incertitudes sur la base du Guide ISO/IEC 98-3. L'Annexe A traite du cas particulier des mesurages répétés par comptage avec des influences aléatoires, alors que l'Annexe B couvre les mesurages avec des ictomètres analogiques linéaires.

NF ISO 11929-2
September 2020
Standard Cancelled
Determination of the characteristic limits (decision threshold, detection limit and limits of the coverage interval) for measurements of ionizing radiation - Fundamentals and application - Part 2 : advanced applications

The ISO 11929 series specifies a procedure, in the field of ionizing radiation metrology, for the calculation of the "decision threshold", the "detection limit" and the "limits of the coverage interval" for a non-negative ionizing radiation measurand when counting measurements with preselection of time or counts are carried out. The measurand results from a gross count rate and a background count rate as well as from further quantities on the basis of a model of the evaluation. In particular, the measurand can be the net count rate as the difference of the gross count rate and the background count rate, or the net activity of a sample. It can also be influenced by calibration of the measuring system, by sample treatment and by other factors. ISO 11929 has been divided into four parts covering elementary applications in ISO 11929-1, advanced applications on the basis of the GUM Supplement 1 in this document, applications to unfolding methods in ISO 11929-3, and guidance to the application in ISO 11929-4. ISO 11929-1 covers basic applications of counting measurements frequently used in the field of ionizing radiation metrology. It is restricted to applications for which the uncertainties can be evaluated on the basis of the ISO/IEC Guide 98-3 (JCGM 2008). In Annex A of ISO 11929-1:2019 the special case of repeated counting measurements with random influences is covered, while measurements with linear analogous ratemeters are covered in Annex B of ISO 11929-1:2019. This document extends the former ISO 11929:2010 to the evaluation of measurement uncertainties according to the ISO/IEC Guide 98-3-1. It also presents some explanatory notes regarding general aspects of counting measurements and on Bayesian statistics in measurements. ISO 11929-3 deals with the evaluation of measurements using unfolding methods and counting spectrometric multi-channel measurements if evaluated by unfolding methods, in particular, for alpha- and gamma‑spectrometric measurements. Further, it provides some advice on how to deal with correlations and covariances. ISO 11929-4 gives guidance to the application of ISO 11929, summarizes shortly the general procedure and then presents a wide range of numerical examples. Information on the statistical roots of ISO 11929 and on its current development may be found elsewhere[30,31]. ISO 11929 also applies analogously to other measurements of any kind especially if a similar model of the evaluation is involved. Further practical examples can be found, for example, in ISO 18589[1], ISO 9696[2], ISO 9697[3], ISO 9698[4], ISO 10703[5], ISO 7503[6], ISO 28218[7], and ISO 11885[8]. NOTE A code system, named UncertRadio, is available for calculations according to ISO 119291 to ISO 11929-3. UncertRadio[27][28] can be downloaded for free from https://www.thuenen.de/en/fi/fields-of-activity/marine-environment/coordination-centre-of-radioactivity/uncertradio/. The download contains a setup installation file which copies all files and folders into a folder specified by the user. After installation one has to add information to the PATH of Windows as indicated by a pop‑up window during installation. English language can be chosen and extensive "help" information is available. . Another tool is the package ?metRology'[32] which is available for programming in R. It contains the two R functions ?uncert' and ?uncertMC' which perform the GUM conform uncertainty propagation, either analytically or by the Monte Carlo method, respectively. Covariances/correlations of input quantities are included. Applying these two functions within iterations for decision threshold and the detection limit calculations simplifies the programming effort significantly. It is also possible to implement this part of ISO 11929 in a spreadsheet containing a Monte Carlo add-in or into other commercial mathematics software.

NF ISO 11929-3
September 2020
Standard Cancelled
Determination of the characteristic limits (decision threshold, detection limit and limits of the coverage interval) for measurements of ionizing radiation - Fundamentals and application - Part 3 : applications to unfolding methods

The ISO 11929 series specifies a procedure, in the field of ionizing radiation metrology, for the calculation of the "decision threshold", the "detection limit" and the "limits of the coverage interval" for a non-negative ionizing radiation measurand when counting measurements with preselection of time or counts are carried out. The measurand results from a gross count rate and a background count rate as well as from further quantities on the basis of a model of the evaluation. In particular, the measurand can be the net count rate as the difference of the gross count rate and the background count rate, or the net activity of a sample. It can also be influenced by calibration of the measuring system, by sample treatment and by other factors. ISO 11929 has been divided into four parts covering elementary applications in ISO 11929-1, advanced applications on the basis of the ISO/IEC Guide 98-3-1 in ISO 11929-2, applications to unfolding methods in this document, and guidance to the application in ISO 11929-4. ISO 11929-1 covers basic applications of counting measurements frequently used in the field of ionizing radiation metrology. It is restricted to applications for which the uncertainties can be evaluated on the basis of the ISO/IEC Guide 98-3 (JCGM 2008). In Annex A of ISO 11929-1:2019, the special case of repeated counting measurements with random influences is covered, while measurements with linear analogous ratemeters, are covered in Annex B of ISO 11929-1:2019. ISO 11929-2 extends the former ISO 11929:2010 to the evaluation of measurement uncertainties according to the ISO/IEC Guide 98-3-1. ISO 11929-2 also presents some explanatory notes regarding general aspects of counting measurements and on Bayesian statistics in measurements. This document deals with the evaluation of measurements using unfolding methods and counting spectrometric multi-channel measurements if evaluated by unfolding methods, in particular, for alpha- and gamma‑spectrometric measurements. Further, it provides some advice on how to deal with correlations and covariances. ISO 11929-4 gives guidance to the application of the ISO 11929 series, summarizes shortly the general procedure and then presents a wide range of numerical examples. ISO 11929 Standard also applies analogously to other measurements of any kind especially if a similar model of the evaluation is involved. Further practical examples can be found, for example, in ISO 18589[7], ISO 9696[2], ISO 9697[3], ISO 9698[4], ISO 10703[5], ISO 7503[1], ISO 28218[8], and ISO 11665[6]. NOTE A code system, named UncertRadio, is available for calculations according to ISO 11929- 1 to ISO 11929-3. UncertRadio[35][36] can be downloaded for free from https://www.thuenen.de/en/fi/fields-of-activity/marine-environment/coordination-centre-of-radioactivity/uncertradio/. The download contains a setup installation file which copies all files and folders into a folder specified by the user. After installation one has to add information to the PATH of Windows as indicated by a pop‑up window during installation. English language can be chosen and extensive "help" information is available.

NF ISO 11929-4
December 2020
Standard Cancelled
Determination of the characteristic limits (decision threshold, detection limit and limits of the coverage interval) for measurements of ionizing radiation - Fundamentals and application - Part 4 : guidelines to applications

This document specifies a procedure, in the field of ionizing radiation metrology, for the calculation of the "decision threshold", the "detection limit" and the "limits of the coverage interval" for a non‑negative ionizing radiation measurand when counting measurements with preselection of time or counts are carried out. The measurand results from a gross count rate and a background count rate as well as from further quantities on the basis of a model of the evaluation. In particular, the measurand can be the net count rate as the difference of the gross count rate and the background count rate, or the net activity of a sample. It can also be influenced by calibration of the measuring system, by sample treatment and by other factors. ISO 11929 has been divided into four parts covering elementary applications in ISO 11929-1, advanced applications on the basis of the ISO/IEC Guide 98-3:2008/Suppl.1 in ISO 11929-2, applications to unfolding methods in ISO 11929-3, and guidance to the application in ISO 11929-4. ISO 11929-1 covers basic applications of counting measurements frequently used in the field of ionizing radiation metrology. It is restricted to applications for which the uncertainties can be evaluated on the basis of the ISO/IEC Guide 98-3 (JCGM 2008). In ISO 11929-1:2019, Annex A the special case of repeated counting measurements with random influences and in ISO 11929-1:2019, Annex B, measurements with linear analogous ratemeters are covered. ISO 11929-2 extends ISO 11929-1 to the evaluation of measurement uncertainties according to the ISO/IEC Guide 98-3:2008/Suppl.1. ISO 11929-2 also presents some explanatory notes regarding general aspects of counting measurements and Bayesian statistics in measurements. ISO 11929-3 deals with the evaluation of measurements using unfolding methods and counting spectrometric multi-channel measurements if evaluated by unfolding methods, in particular, alpha- and gamma-spectrometric measurements. Further, it provides some advice how to deal with correlations and covariances. ISO 11929-4 gives guidance to the application of ISO 11929 (all parts), summarizing shortly the general procedure and then presenting a wide range of numerical examples. The examples cover elementary applications according to ISO 11929-1 and ISO 11929-2. The ISO 11929 (all parts) also applies analogously to other measurements of any kind if a similar model of the evaluation is involved. Further practical examples can be found in other International Standards, for example, see References [1 to 20].

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Table of contents
  • Avant-propos
    iv
  • Introduction
    v
  • 1 Domaine d'application
    1
  • 2 Références normatives
    2
  • 3 Termes et définitions
    2
  • 4 Grandeurs et symboles
    4
  • 5 Principes essentiels
    6
  • 5.1 Aspects généraux concernant le mesurande
    6
  • 5.2 Modèle
    6
  • 5.3 Calcul de l'incertitude-type comme fonction du mesurande
    8
  • 6 Limites et évaluations caractéristiques
    10
  • 6.1 Spécifications
    10
  • 6.2 Seuil de décision
    10
  • 6.3 Limite de détection
    10
  • 6.4 Extrémités de l'intervalle de confiance
    12
  • 6.5 Évaluation du résultat de mesurage
    13
  • 6.6 Évaluation de la procédure de mesure
    14
  • 7 Documentation
    15
  • Annexe A (informative) Vue d'ensemble de la procédure générale
    16
  • Annexe B (normative) Applications diverses
    18
  • Annexe C (normative) Applications à des mesures par comptage spectrométriques
    25
  • Annexe D (informative) Exemples d'application
    38
  • Annexe E (informative) Fonction de distribution de la distribution normale type
    50
  • Annexe F (informative) Notes explicatives
    52
  • Bibliographie
    60
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