NF ISO 13160

NF ISO 13160

October 2012
Standard Cancelled

Water quality - Strontium 90 and strontium 89 - Test methods using liquid scintillation counting or proportional counting

ISO 13160:2012 specifies the test methods and their associated principles for the measurement of the activity of 90Sr in equilibrium with 90Y, and 89Sr, pure beta-emitting radionuclides, in water samples. Different chemical separation methods are presented to produce strontium and yttrium sources, the activity of which is determined using a proportional counter (PC) or liquid scintillation counter (LSC). The selection of the test method depends on the origin of the contamination, the characteristics of the water to be analysed, the required accuracy of test results and the available resources of the laboratories.These test methods are used for water monitoring following, past or present, accidental or routine, liquid or gaseous discharges. It also covers the monitoring of contamination caused by global fallout.When fallout occurs immediately following a nuclear accident, the contribution of 89Sr to the total amount of strontium activity is not negligible. ISO 13160:2012 provides the test methods to determine the activity concentration of 90Sr in presence of 89Sr.

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Main informations

Collections

National standards and national normative documents

Publication date

October 2012

Number of pages

45 p.

Reference

NF ISO 13160

ICS Codes

13.060.60   Examination of physical properties of water
17.240   Radiation measurements
27.120.01   Nuclear energy in general

Classification index

M60-806

Print number

1 - 28/09/2012

International kinship

Sumary
Water quality - Strontium 90 and strontium 89 - Test methods using liquid scintillation counting or proportional counting

ISO 13160:2012 specifies the test methods and their associated principles for the measurement of the activity of 90Sr in equilibrium with 90Y, and 89Sr, pure beta-emitting radionuclides, in water samples. Different chemical separation methods are presented to produce strontium and yttrium sources, the activity of which is determined using a proportional counter (PC) or liquid scintillation counter (LSC). The selection of the test method depends on the origin of the contamination, the characteristics of the water to be analysed, the required accuracy of test results and the available resources of the laboratories.

These test methods are used for water monitoring following, past or present, accidental or routine, liquid or gaseous discharges. It also covers the monitoring of contamination caused by global fallout.

When fallout occurs immediately following a nuclear accident, the contribution of 89Sr to the total amount of strontium activity is not negligible. ISO 13160:2012 provides the test methods to determine the activity concentration of 90Sr in presence of 89Sr.

Replaced standards (3)
NF M60-806-1
May 2005
Standard Cancelled
Nuclear energy - Measurement of radioactivity in the environment - Water - Part 1 : measurement of strontium 90 activity in water - Radiochemical separation of strontium by nitric acid and measurement of yttrium 90 beta activity

Le présent document décrit les conditions de mesurage du strontium 90 par la méthode d'extraction par l'acide nitrique fumant et comptage par compteur à circulation gazeuse.

NF M60-806-2
May 2005
Standard Cancelled
Nuclear energy - Measurement of radioactivity in the environment - Water - Part 2 : measurement of strontium 90 activity in water - organic solvent extraction of yttrium 90 and measurement of beta activity

Le présent document décrit les conditions de mesurage du strontium 90 par la méthode d'extraction de l'yttrium.

NF M60-806-3
May 2005
Standard Cancelled
Nuclear energy - Measurement of radioactivity in the environment - Water - Part 3 : measurement of strontium 90 activity in water - Radiochemical separation of strontium by extraction with "ethers crown" resin and measurement of beta activity

Le présent document décrit les conditions de mesurage de l'activité du strontium 90, avec une séparation radiochimique du strontium 90 par extraction sur résine de type "éther-couronne".

Standard replaced by (1)
NF EN ISO 13160
February 2016
Standard Cancelled
Water quality - Strontium 90 and strontium 89 - Test methods using liquid scintillation counting or proportional counting

ISO 13160:2012 specifies the test methods and their associated principles for the measurement of the activity of 90Sr in equilibrium with 90Y, and 89Sr, pure beta-emitting radionuclides, in water samples. Different chemical separation methods are presented to produce strontium and yttrium sources, the activity of which is determined using a proportional counter (PC) or liquid scintillation counter (LSC). The selection of the test method depends on the origin of the contamination, the characteristics of the water to be analysed, the required accuracy of test results and the available resources of the laboratories. These test methods are used for water monitoring following, past or present, accidental or routine, liquid or gaseous discharges. It also covers the monitoring of contamination caused by global fallout. When fallout occurs immediately following a nuclear accident, the contribution of 89Sr to the total amount of strontium activity is not negligible. ISO 13160:2012 provides the test methods to determine the activity concentration of 90Sr in presence of 89Sr.

Table of contents
  • Avant-propos
    iv
  • 1 Domaine d'application
    1
  • 2 Références normatives
    1
  • 3 Symboles, définitions et unités
    1
  • 4 Principe
    2
  • 4.1 Généralités
    2
  • 4.2 Séparation chimique
    3
  • 4.3 Détection
    3
  • 5 Réactifs chimiques et appareillage
    3
  • 6 Mode opératoire
    3
  • 6.1 Préparation de la prise d'essai
    3
  • 6.2 Séparation chimique
    4
  • 6.3 Préparation de la source pour essai
    5
  • 6.4 Mesurage
    6
  • 7 Expression des résultats
    8
  • 7.1 Détermination de 90Sr en équilibre avec 90Y
    8
  • 7.2 Détermination de 90Sr par croissance du 90Y
    9
  • 7.3 Détermination de 90Sr en présence de 89Sr lorsque le 90Sr et le 90Y sont en équilibre
    11
  • 7.4 Limites de l'intervalle de confiance
    14
  • 8 Contrôle de la qualité
    14
  • 9 Rapport d'essai
    14
  • Annexe A (informative) Détermination de 89Sr et 90Sr par précipitation et comptage proportionnel
    16
  • Annexe B (informative) Détermination de 89Sr et 90Sr par précipitation et comptage des scintillations en milieu liquide
    20
  • Annexe C (informative) Détermination de 90Sr à partir de son produit de filiation 90Y en équilibre, par extraction organique et comptage des scintillations en milieu liquide
    24
  • Annexe D (informative) Détermination de 90Sr après séparation par échange d'ions, par comptage proportionnel
    27
  • Annexe E (informative) Détermination de 90Sr après séparation sur une résine spécifique de type "éther couronne" et comptage des scintillations en milieu liquide
    30
  • Annexe F (informative) Détermination de 90Sr à partir de son produit de filiation 90Y en équilibre par extraction organique et comptage proportionnel
    32
  • Annexe G (informative) Facteur de correction relatif au contrôle de la pureté en utilisant le comptage proportionnel
    36
  • Bibliographie
    39
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