NF ISO 22634-1
Cigarettes - Determination of benzo[a]pyrene in cigarette mainstream smoke using GC/MS - Part 1 : Method using methanol as extraction solvent
ISO 22634-1:2017 specifies a method for the determination of benzo[a]pyrene (B[a]P) in the total particulate matter of cigarette mainstream smoke using gas chromatography/mass spectrometry (GC/MS) with methanol as extraction solvent.This method was validated using ISO 3308 smoking parameters and is technically compatible with other smoking regimes. An alternative method for the determination of B[a]P is specified in ISO 22634‑2 with a different clean-up using cyclohexane solvent and a reduced analytical run.
ISO 22634-1:2017 specifies a method for the determination of benzo[a]pyrene (B[a]P) in the total particulate matter of cigarette mainstream smoke using gas chromatography/mass spectrometry (GC/MS) with methanol as extraction solvent.
This method was validated using ISO 3308 smoking parameters and is technically compatible with other smoking regimes.
An alternative method for the determination of B[a]P is specified in ISO 22634‑2 with a different clean-up using cyclohexane solvent and a reduced analytical run.
ISO 22634:2008 specifies a method for the determination of benzo[a]pyrene (B[a]P) in the total particulate matter of cigarette mainstream smoke. This method is specified using ISO 3308 smoking parameters, but is technically compatible with other smoking regimes.
This document specifies a method for the determination of benzo[a]pyrene (B[a]P) in the total particulate matter (TPM) of cigarette mainstream smoke using gas chromatography/mass spectrometry (GC/MS) with methanol as extraction solvent. This method is specified using ISO 3308 smoking parameters. An alternative method for the determination of B[a]P is specified in ISO 22634-2 with a different clean-up using cyclohexane solvent and a shorter total analytical time.
- Avant-propos
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1 Domaine d'application
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2 Références normatives
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3 Termes et définitions
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4 Principe
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5 Appareillage
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6 Réactifs
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7 Étalons
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8 Préparation de l'échantillon
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9 Dosage
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10 Répétabilité et reproductibilité
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11 Rapport d'essai
- Annexe A (informative) Exemple de chromatogramme d'un extrait de fumée de cigarette
- Bibliographie
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