NF ISO 22634-1

NF ISO 22634-1

May 2020
Standard Current

Cigarettes - Determination of benzo[a]pyrene in cigarette mainstream smoke using GC/MS - Part 1 : method using methanol as extraction solvent

This document specifies a method for the determination of benzo[a]pyrene (B[a]P) in the total particulate matter (TPM) of cigarette mainstream smoke using gas chromatography/mass spectrometry (GC/MS) with methanol as extraction solvent.This method is specified using ISO 3308 smoking parameters. An alternative method for the determination of B[a]P is specified in ISO 22634-2 with a different clean-up using cyclohexane solvent and a shorter total analytical time.

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Main informations

Collections

National standards and national normative documents

Publication date

May 2020

Number of pages

17 p.

Reference

NF ISO 22634-1

ICS Codes

65.160   Tobacco, tobacco products and related equipment

Classification index

V37-050-1

Print number

1

International kinship

ISO 22634-1:2019
Sumary
Cigarettes - Determination of benzo[a]pyrene in cigarette mainstream smoke using GC/MS - Part 1 : method using methanol as extraction solvent

This document specifies a method for the determination of benzo[a]pyrene (B[a]P) in the total particulate matter (TPM) of cigarette mainstream smoke using gas chromatography/mass spectrometry (GC/MS) with methanol as extraction solvent.

This method is specified using ISO 3308 smoking parameters. An alternative method for the determination of B[a]P is specified in ISO 22634-2 with a different clean-up using cyclohexane solvent and a shorter total analytical time.

Replaced standards (1)
NF ISO 22634-1
January 2018
Standard Cancelled
Cigarettes - Determination of benzo[a]pyrene in cigarette mainstream smoke using GC/MS - Part 1 : Method using methanol as extraction solvent

ISO 22634-1:2017 specifies a method for the determination of benzo[a]pyrene (B[a]P) in the total particulate matter of cigarette mainstream smoke using gas chromatography/mass spectrometry (GC/MS) with methanol as extraction solvent. This method was validated using ISO 3308 smoking parameters and is technically compatible with other smoking regimes. An alternative method for the determination of B[a]P is specified in ISO 22634‑2 with a different clean-up using cyclohexane solvent and a reduced analytical run.

Table of contents
  • 1 Domaine d'application
  • 2 Références normatives
  • 3 Termes et définitions
  • 4 Principe
  • 5 Appareillage
  • 6 Réactifs
  • 7 Étalons
  • 8 Préparation de l'échantillon
  • 9 Dosage
  • 10 Répétabilité et reproductibilité
  • 11 Rapport d'essai
  • Annexe A Exemple de chromatogramme d'un extrait de fumée de cigarette
  • Bibliographie
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