XP ISO/TS 19036
Microbiology of food and animal feeding stuffs - Guidelines for the estimation measurement uncertainty for quantitative determinations
ISO/TS 19036:2006 gives guidance for the estimation and expression of measurement uncertainty (MU) associated with quantitative results in food microbiology. It is applicable to the quantitative analysis of products intended for human consumption and the feeding of animals, and of environmental samples in the area of food production and food handling, typically carried out by enumeration of microorganisms using a colony-count technique, but applicable also to quantitative analysis by alternative instrumental methods.ISO/TS 19036:2006 is not applicable to enumeration using a most probable number technique, or the analysis of low levels of microorganisms.
ISO/TS 19036:2006 gives guidance for the estimation and expression of measurement uncertainty (MU) associated with quantitative results in food microbiology.
It is applicable to the quantitative analysis of products intended for human consumption and the feeding of animals, and of environmental samples in the area of food production and food handling, typically carried out by enumeration of microorganisms using a colony-count technique, but applicable also to quantitative analysis by alternative instrumental methods.
ISO/TS 19036:2006 is not applicable to enumeration using a most probable number technique, or the analysis of low levels of microorganisms.
This document specifies requirements and gives guidance for the estimation and expression of measurement uncertainty (MU) associated with quantitative results in microbiology of the food chain. It is applicable to the quantitative analysis of: — products intended for human consumption or the feeding of animals; — environmental samples in the area of food production and food handling; — samples at the stage of primary production. The quantitative analysis is typically carried out by enumeration of microorganisms using a colony-count technique. This document is also generally applicable to other quantitative analyses, including: — most probable number (MPN) techniques; — instrumental methods, such as impediometry, adenosine triphosphate (ATP) and flow cytometry; — molecular methods, such as methods based on quantitative polymerase chain reaction (qPCR). The uncertainty estimated by this document does not include systematic effects (bias).
- Avant-proposiv
- Introductionv
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1 Domaine d'application1
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2 Termes et définitions1
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3 Principes3
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3.1 Approche globale de l'estimation de l'incertitude de mesure (IM)3
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3.2 Prise en considération du biais4
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4 Aspects généraux4
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4.1 Incertitude type composée4
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4.2 Écart-type de reproductibilité4
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4.3 Incertitude élargie5
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4.4 Règles générales d'estimation de l'écart-type de reproductibilité5
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5 Écart-type de reproductibilité intralaboratoire5
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5.1 Généralités5
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5.2 Protocole expérimental5
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5.3 Calculs8
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6 Écart-type de reproductibilité de la méthode dérivé d'un essai interlaboratoires9
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6.1 Généralités9
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6.2 Utilisation en microbiologie des aliments10
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7 Écart-type de reproductibilité dérivé d'un essai interlaboratoires d'aptitude11
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8 Expression de l'incertitude de mesure dans les rapports d'essai11
- Annexe A (informative) Résultats des essais concernant la composante d'incertitude liée au sous-échantillonnage de la prise d'essai et à la préparation de la suspension mère12
- Bibliographie17
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